Organometallic Compounds
173
with Grignard reagent, and gas chromatographic analysis using flame photometric
detection. Recoveries from fish samples spiked at 0.2 and 1.0 mg kg-I were 80-104 %
(i. e. 92 ± 12 %) for tri-n-butyltin and 92-105 % (i. e. 98 ± 6 %) for di-n-butyltin.
The detection limit for both compounds was 0.2 mg kg-I. The levels determined in
reared yellowtail fish were similar for both flame photometric detection gas chromatography and gas chromatography mass spectrometry.
173
with Grignard reagent, and gas chromatographic analysis using flame photometric
detection. Recoveries from fish samples spiked at 0.2 and 1.0 mg kg-I were 80-104 %
(i. e. 92 ± 12 %) for tri-n-butyltin and 92-105 % (i. e. 98 ± 6 %) for di-n-butyltin.
The detection limit for both compounds was 0.2 mg kg-I. The levels determined in
reared yellowtail fish were similar for both flame photometric detection gas chromatography and gas chromatography mass spectrometry.