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from micro-precipitation in molten stearic acid,” Journal of Power Sources, vol. 124, no. 1,
pp. 118–123, 2003.
69. A. R. Naghash and J. Y. Lee, “Preparation of spinel lithium manganese oxide by aqueous
co-precipitation,” Journal of Power Sources, vol. 85, no. 2, pp. 284–293, 2000.
70. E. Antolini “Lithium loss kinetics from polycrystalline Li x Ni 1−x O at high temperatures,”
Journal of Materials Chemistry, vol. 8, no. 12, pp. 2783–2786, 1998.
71. J. B. Goodenough, D. G. Wickham, and W. J. Croft “Some magnetic and crystallographic
properties of the system Li
+
x Ni
++
1−2x Ni
+++
x
O,” Journal of Physics and Chemistry of Solids,
vol. 5, no. 1, pp. 107–116, 1958.
72. R. Gunawan and D. Zhang, “Thermal stability and kinetics of decomposition of ammonium
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73. R. D. Vold and G. S. Hattiangdi, “Characterization of heavy metal soaps by X-ray diffraction,”
Industrial & Engineering Chemistry, vol. 41, no. 10, pp. 2311–2320, 1949.
74. V. Berbenni and A. Marini, “Thermogravimetry and X-ray diffraction study of the thermal
decomposition processes in Li 2 CO 3 –MnCO 3 mixtures,” Journal of Analytical and Applied
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75. E. McCalla, C. M. Lowartz, C. R. Brown, and J. R. Dahn “Formation of layered-layered
composites in the Li-Co-Mn oxide pseudoternary system during slow cooling,” Chemistry of
Materials, vol. 25, no. 6, pp. 912–918, 2013.
76. C. R. Brown, E. McCalla, and J. R. Dahn “Analysis of the cubic spinel region of the Li-Co-Mn
oxide pseudo-ternary system,” accepted by Solid State Ionics, 2013.
77. S. Levasseur, M. Menetrier, E. Suard, and C. Delmas “Evidence for structural defects in nonstoichiometric HT-LiCoO 2 : electrochemical, electronic properties and
7 Li NMR studies,”
Solid State Ionics, vol. 128, no. 1, pp. 11–24, 2000.
78. Y. Sun,Y. Shiosaki,Y. Xia, and H. Noguchi “The preparation and electrochemical performance
of solid solutions LiCoO 2 -Li 2 MnO 3 as cathode materials for lithium ion batteries,” Journal
of Power Sources, vol. 159, no. 2, pp. 1353–1359, 2006.
79. A. Van der Ven, M. K. Aydinol, G. Ceder, G. Kresse, and J. Hafner, “First-principles investigation of phase stability in Li x CoO 2 ,” Physical Review B, vol. 58, no. 6, p. 2975,
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80. E. McCalla and J. R. Dahn, “The spinel and cubic rocksalt solid-solutions in the Li-Mn-Ni
oxide pseudo-ternary system,” Solid State Ionics, vol. 242, pp. 1–9, 2013.
81. J. S. Kasper and J. S. Prener, “The crystal structure of Mg 6 MnO 8 ,” Acta Crystallographica,
vol. 7, no. 3, pp. 246–248, 1954.
82. G. W. Brindley “The effect of grain or particle size on X-ray reflections from mixed powders
and alloys, considered in relation to the quantitative determination of crystalline substances
by X-ray methods,” Philosophical Magazine, vol. 36, no. 256, pp. 347–369, 1945.
83. B. J. Neudecker, R. A. Zuhr, B. S. Kwak, J. B. Bates, and J. D. Robertson “Lithium manganese
nickel oxides Li x (Mn y Ni 1−y ) 2−x O 2 i. synthesis and characterization of thin films and bulk
phases,” Journal of the Electrochemical Society, vol. 145, no. 12, pp. 4148–4159, 1998.
84. E. McCalla, A. W. Rowe, C. R. Brown, L. R. P. Hacquebard, and J. R. Dahn “How phase
transformations during cooling affect Li-Mn-Ni-O positive electrodes in lithium ion batteries,”
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86. T. Ohzuku, and Y. Makimura, “Layered lithium insertion material of LiNi 1/2 Mn 1/2 O 2 : a
possible alternative to LiCoO 2 for advanced lithium-ion batteries,” Chemistry Letters, vol. 30,
no. 8, pp. 744–745, 2001.
87. C. R. Fell, D. Qian, K. J. Carroll, M. Chi, J. L. Jones, and Y. S. Meng “Correlation between
oxygen vacancy, microstrain, and cation distribution in lithium-excess layered oxides during
the first electrochemical cycle,” Chemistry of Materials, vol. 25, no. 9, pp. 1621–1629, 2013.
143
68. S. M. Lala, L. A. Montoro, and J. M. Rosolen, “LiCoO 2 sub-microns particles obtained
from micro-precipitation in molten stearic acid,” Journal of Power Sources, vol. 124, no. 1,
pp. 118–123, 2003.
69. A. R. Naghash and J. Y. Lee, “Preparation of spinel lithium manganese oxide by aqueous
co-precipitation,” Journal of Power Sources, vol. 85, no. 2, pp. 284–293, 2000.
70. E. Antolini “Lithium loss kinetics from polycrystalline Li x Ni 1−x O at high temperatures,”
Journal of Materials Chemistry, vol. 8, no. 12, pp. 2783–2786, 1998.
71. J. B. Goodenough, D. G. Wickham, and W. J. Croft “Some magnetic and crystallographic
properties of the system Li
+
x Ni
++
1−2x Ni
+++
x
O,” Journal of Physics and Chemistry of Solids,
vol. 5, no. 1, pp. 107–116, 1958.
72. R. Gunawan and D. Zhang, “Thermal stability and kinetics of decomposition of ammonium
nitrate in the presence of pyrite,” Journal of Hazardous Materials, vol. 165, no. 1, pp. 751–758,
2009.
73. R. D. Vold and G. S. Hattiangdi, “Characterization of heavy metal soaps by X-ray diffraction,”
Industrial & Engineering Chemistry, vol. 41, no. 10, pp. 2311–2320, 1949.
74. V. Berbenni and A. Marini, “Thermogravimetry and X-ray diffraction study of the thermal
decomposition processes in Li 2 CO 3 –MnCO 3 mixtures,” Journal of Analytical and Applied
Pyrolysis, vol. 62, no. 1, pp. 45–62, 2002.
75. E. McCalla, C. M. Lowartz, C. R. Brown, and J. R. Dahn “Formation of layered-layered
composites in the Li-Co-Mn oxide pseudoternary system during slow cooling,” Chemistry of
Materials, vol. 25, no. 6, pp. 912–918, 2013.
76. C. R. Brown, E. McCalla, and J. R. Dahn “Analysis of the cubic spinel region of the Li-Co-Mn
oxide pseudo-ternary system,” accepted by Solid State Ionics, 2013.
77. S. Levasseur, M. Menetrier, E. Suard, and C. Delmas “Evidence for structural defects in nonstoichiometric HT-LiCoO 2 : electrochemical, electronic properties and
7 Li NMR studies,”
Solid State Ionics, vol. 128, no. 1, pp. 11–24, 2000.
78. Y. Sun,Y. Shiosaki,Y. Xia, and H. Noguchi “The preparation and electrochemical performance
of solid solutions LiCoO 2 -Li 2 MnO 3 as cathode materials for lithium ion batteries,” Journal
of Power Sources, vol. 159, no. 2, pp. 1353–1359, 2006.
79. A. Van der Ven, M. K. Aydinol, G. Ceder, G. Kresse, and J. Hafner, “First-principles investigation of phase stability in Li x CoO 2 ,” Physical Review B, vol. 58, no. 6, p. 2975,
1998.
80. E. McCalla and J. R. Dahn, “The spinel and cubic rocksalt solid-solutions in the Li-Mn-Ni
oxide pseudo-ternary system,” Solid State Ionics, vol. 242, pp. 1–9, 2013.
81. J. S. Kasper and J. S. Prener, “The crystal structure of Mg 6 MnO 8 ,” Acta Crystallographica,
vol. 7, no. 3, pp. 246–248, 1954.
82. G. W. Brindley “The effect of grain or particle size on X-ray reflections from mixed powders
and alloys, considered in relation to the quantitative determination of crystalline substances
by X-ray methods,” Philosophical Magazine, vol. 36, no. 256, pp. 347–369, 1945.
83. B. J. Neudecker, R. A. Zuhr, B. S. Kwak, J. B. Bates, and J. D. Robertson “Lithium manganese
nickel oxides Li x (Mn y Ni 1−y ) 2−x O 2 i. synthesis and characterization of thin films and bulk
phases,” Journal of the Electrochemical Society, vol. 145, no. 12, pp. 4148–4159, 1998.
84. E. McCalla, A. W. Rowe, C. R. Brown, L. R. P. Hacquebard, and J. R. Dahn “How phase
transformations during cooling affect Li-Mn-Ni-O positive electrodes in lithium ion batteries,”
Journal of The Electrochemical Society, vol. 160, no. 8, pp. A1134–A1138, 2013.
85. F. N. Rhines, Phase Diagrams in Metallurgy. New York: McGraw-Hill., 1956.
86. T. Ohzuku, and Y. Makimura, “Layered lithium insertion material of LiNi 1/2 Mn 1/2 O 2 : a
possible alternative to LiCoO 2 for advanced lithium-ion batteries,” Chemistry Letters, vol. 30,
no. 8, pp. 744–745, 2001.
87. C. R. Fell, D. Qian, K. J. Carroll, M. Chi, J. L. Jones, and Y. S. Meng “Correlation between
oxygen vacancy, microstrain, and cation distribution in lithium-excess layered oxides during
the first electrochemical cycle,” Chemistry of Materials, vol. 25, no. 9, pp. 1621–1629, 2013.