Gao H, Xu R, Cao W, Qian L, Wang M, Lu L, Xu Q, Yu S (2017) Effects of six priority controlled
phthalate esters with long-term low-dose integrated exposure on male reproductive toxicity in
rats. Food Chem Toxicol 101:94–104. https://doi.org/10.1016/j.fct.2017.01.011
Gao D, Li Z, Wang H, Liang H (2018) An overview of phthalate acid ester pollution in China over
the last decade: environmental occurrence and human exposure. Sci Total Environ
645:1400–1409. https://doi.org/10.1016/j.scitotenv.2018.07.093
Gao X, Li J, Wang X, Zhou J, Fan B, Li W, Liu Z (2019) Exposure and ecological risk of phthalate
esters in the Taihu Lake basin, China. Ecotox Environ Safe 171:564–570. https://doi.org/10.
1016/j.ecoenv.2019.01.001
González-Sálamo J, González-Curbelo M, Socas-Rodríguez M, Hernández-Borges J, RodríguezDelgado M (2018) Determination of phthalic acid esters in water samples by hollow fiber liquidphase microextraction prior to gas chromatography tandem mass spectrometry. Chemosphere
201:254–261. https://doi.org/10.1016/j.chemosphere.2018.02.180
González-Sálamo J, González-Curbelo M, Hernández-Borges J, Rodríguez-Delgado M (2019) Use
of Basolite® F300 metal-organic framework for the dispersive solid-phase extraction of phthalic
acid esters from water samples prior to LC-MS determination. Talanta 195:236–244. https://doi.
org/10.1016/j.talanta.2018.11.049
Guo L, Lee H (2013) Vortex-assisted micro-solid-phase extraction followed by low-density solvent
based dispersive liquid–liquid microextraction for the fast and efficient determination of phthalate esters in river water samples. J Chromatogr A 1300:24–30. https://doi.org/10.1016/j.chroma.
2013.01.030
Guo L, Ma X, Xie X, Huang R, Zhang M, Li J, Zeng G, Fan Y (2019a) Preparation of dual-dummytemplate molecularly imprinted polymers coated magnetic graphene oxide for separation and
enrichment of phthalate esters in water. Chem Eng J 361:245–255. https://doi.org/10.1016/j.cej.
2018.12.076
Guo H, Song N, Wang D, Ma J, Jia Q (2019b) A modulation approach for covalent organic
frameworks: application to solid phase microextraction of phthalate esters. Talanta
198:277–283. https://doi.org/10.1016/j.talanta.2019.02.025
He J, Lv R, Zhan H, Wang H, Cheng J, Lu K, Wang F (2010) Preparation and evaluation of
molecularly imprinted solid-phase micro-extraction fibers for selective extraction of phthalates
in an aqueous sample. Anal Chim Acta 674(1):53–58. https://doi.org/10.1016/j.aca.2010.06.018
Herreros M, Encinas T, Torres-Rovira L, Garcia-Fernandez R, Flores J, Ros J, Gonzalez-Bulnes A
(2013) Exposure to the endocrine disruptor di(2-ethylhexyl)phthalate affects female reproductive features by altering pulsatile LH secretion. Environ Toxicol Pharmacol 36(3):1141–1149.
https://doi.org/10.1016/j.etap.2013.09.020
Huang G, Li H, Zhang B, Ma Y, Lin J (2012) Vortex solvent bar microextraction for phthalate
esters from aqueous matrices. Talanta 100:64–70. https://doi.org/10.1016/j.talanta.2012.08.009
Huysman S, Van Meulebroek L, Janssens O, Vanryckeghem F, Van Langenhove H, Demeestere K,
Vanhaecke L (2019) Targeted quantification and untargeted screening of alkylphenols,
bisphenol A and phthalates in aquatic matrices using ultra-high-performance liquid chromatography coupled to hybrid Q-Orbitrap mass spectrometry. Anal Chim Acta 1049:141–151. https://
doi.org/10.1016/j.aca.2018.10.045
Jeannot M, Cantwell F (1996) Solvent microextraction into a single drop. Anal Chem 68
(13):2236–2240. https://doi.org/10.1021/ac960042z
Jeannot M, Cantwell F (1997) Solvent microextraction as a speciation tool: determination of free
progesterone in a protein solution. Anal Chem 69(15):2935–2940. https://doi.org/10.1021/
ac970207j
Jia N, Xu H, Hu Y, Lin X, Chen M, Zhang S, Wang G, Ren R (2005) Determination of the
phthalates in water samples in Beijing city by solid-phase extraction and gas chromatography.
Chin J Anal Lab 11:23–26(in Chinese). https://doi.org/10.13595/j.cnki.issn1000-0720.2005.
0253
570
C. Sun et al.
phthalate esters with long-term low-dose integrated exposure on male reproductive toxicity in
rats. Food Chem Toxicol 101:94–104. https://doi.org/10.1016/j.fct.2017.01.011
Gao D, Li Z, Wang H, Liang H (2018) An overview of phthalate acid ester pollution in China over
the last decade: environmental occurrence and human exposure. Sci Total Environ
645:1400–1409. https://doi.org/10.1016/j.scitotenv.2018.07.093
Gao X, Li J, Wang X, Zhou J, Fan B, Li W, Liu Z (2019) Exposure and ecological risk of phthalate
esters in the Taihu Lake basin, China. Ecotox Environ Safe 171:564–570. https://doi.org/10.
1016/j.ecoenv.2019.01.001
González-Sálamo J, González-Curbelo M, Socas-Rodríguez M, Hernández-Borges J, RodríguezDelgado M (2018) Determination of phthalic acid esters in water samples by hollow fiber liquidphase microextraction prior to gas chromatography tandem mass spectrometry. Chemosphere
201:254–261. https://doi.org/10.1016/j.chemosphere.2018.02.180
González-Sálamo J, González-Curbelo M, Hernández-Borges J, Rodríguez-Delgado M (2019) Use
of Basolite® F300 metal-organic framework for the dispersive solid-phase extraction of phthalic
acid esters from water samples prior to LC-MS determination. Talanta 195:236–244. https://doi.
org/10.1016/j.talanta.2018.11.049
Guo L, Lee H (2013) Vortex-assisted micro-solid-phase extraction followed by low-density solvent
based dispersive liquid–liquid microextraction for the fast and efficient determination of phthalate esters in river water samples. J Chromatogr A 1300:24–30. https://doi.org/10.1016/j.chroma.
2013.01.030
Guo L, Ma X, Xie X, Huang R, Zhang M, Li J, Zeng G, Fan Y (2019a) Preparation of dual-dummytemplate molecularly imprinted polymers coated magnetic graphene oxide for separation and
enrichment of phthalate esters in water. Chem Eng J 361:245–255. https://doi.org/10.1016/j.cej.
2018.12.076
Guo H, Song N, Wang D, Ma J, Jia Q (2019b) A modulation approach for covalent organic
frameworks: application to solid phase microextraction of phthalate esters. Talanta
198:277–283. https://doi.org/10.1016/j.talanta.2019.02.025
He J, Lv R, Zhan H, Wang H, Cheng J, Lu K, Wang F (2010) Preparation and evaluation of
molecularly imprinted solid-phase micro-extraction fibers for selective extraction of phthalates
in an aqueous sample. Anal Chim Acta 674(1):53–58. https://doi.org/10.1016/j.aca.2010.06.018
Herreros M, Encinas T, Torres-Rovira L, Garcia-Fernandez R, Flores J, Ros J, Gonzalez-Bulnes A
(2013) Exposure to the endocrine disruptor di(2-ethylhexyl)phthalate affects female reproductive features by altering pulsatile LH secretion. Environ Toxicol Pharmacol 36(3):1141–1149.
https://doi.org/10.1016/j.etap.2013.09.020
Huang G, Li H, Zhang B, Ma Y, Lin J (2012) Vortex solvent bar microextraction for phthalate
esters from aqueous matrices. Talanta 100:64–70. https://doi.org/10.1016/j.talanta.2012.08.009
Huysman S, Van Meulebroek L, Janssens O, Vanryckeghem F, Van Langenhove H, Demeestere K,
Vanhaecke L (2019) Targeted quantification and untargeted screening of alkylphenols,
bisphenol A and phthalates in aquatic matrices using ultra-high-performance liquid chromatography coupled to hybrid Q-Orbitrap mass spectrometry. Anal Chim Acta 1049:141–151. https://
doi.org/10.1016/j.aca.2018.10.045
Jeannot M, Cantwell F (1996) Solvent microextraction into a single drop. Anal Chem 68
(13):2236–2240. https://doi.org/10.1021/ac960042z
Jeannot M, Cantwell F (1997) Solvent microextraction as a speciation tool: determination of free
progesterone in a protein solution. Anal Chem 69(15):2935–2940. https://doi.org/10.1021/
ac970207j
Jia N, Xu H, Hu Y, Lin X, Chen M, Zhang S, Wang G, Ren R (2005) Determination of the
phthalates in water samples in Beijing city by solid-phase extraction and gas chromatography.
Chin J Anal Lab 11:23–26(in Chinese). https://doi.org/10.13595/j.cnki.issn1000-0720.2005.
0253
570
C. Sun et al.