8
Solid-phase microextraction
Drinking water
Ultrahigh-performance liquid
chromatography-ultraviolet
detection;
Column:C18
(350 mm
 100 mm, 3.0
μm)
Recovery:75.5–99.7%;
LODs:0.18–2.95
μg/L;
RSDs:<6.2%
Lirio et al. (2016)
7
Solid-phase microextraction
Drinking water
Gas chromatography–tandem
mass spectrometry;
Column: HP-5MS
(30 m
 0.20 mm, 0.25
μm)
LODs:0.005–0.04
μg/L;
RSDs:4.4–28.3%
Luks-Betlej et al.
(2001)
11 + 9
monophthalates
Solid-phase extraction
Seawater and fresh
water
Ultrahigh-performance liquid
chromatography-Orbitrapmass spectrometry;
Column:Hypersil gold
(100 mm
 1.9 mm, 2.1
μm)
Recovery:98.5–105.8%
LODs:5-25 ng/L;
RSDs:<10%
Huysman et al.
(2019)
9
Dispersive solid-phase extraction
Tap water, pond
water, and wastewater
Ultrahigh-performance liquid
chromatography-tandem
mass spectrometry;
Column: C18
(100 mm
 4.6 mm, 3.5
μm)
Recovery:70–118%;
LODs:0.024–0.069
μg/L;
RSDs:<20%
González-Sálamo
et al. (2019)
5
Air-assisted liquid–liquid
microextraction
Bottled and mineral
water
Gas chromatography-flame
ionization detection;
Column:HP-5 MS
(30 m
 0.25 mm.,0.25μm)
Recovery:91–104%;
LODs:0.12–1.15
μg/L;
RSDs:2–3%
Farajzadeh and
Mogaddam
(2012)
3
Dispersive liquid–liquid
microextraction
Lake, tap, and bottled water
High-performance liquid
chromatography-ultraviolet
detection;
Column:C8
(150mm
 4.6 mm,5μm)
Recovery:84–113%;
LODs:0.64–1.8ug/L;
RSDs:3.1–6.8%
Liang et al.
(2008)
(continued)
15 Analytical Methods for Phthalates in Water Samples
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