Table 15.2
(continued)
Number of
phthalates
detected
Sample treatment method
Sample matrix
Separation and detection
method
Method performance
References
16
Solid-phase microextraction
Tap water and lake
water
Gas chromatography–tandem
mass spectrometry;
Column: TG-5MS
(30 m
 0.25 mm, 0.25μ m)
Recovery:80.4% -
108.2%;
LODs:0.006–0.021μg/L;
RSDs:<12.8%
Zhao et al. (2016)
7
Solid-phase microextraction
Tap water
Gas chromatography–tandem
mass spectrometry;
Column: HP-5MS
(30 m
 250 mm,0.25 mm)
Recovery:91.1–113.4%;
LODs:0.006–0.068μg/L;
RSDs:3.4–11.7%
Meng et al.
(2011)
14
Magnetic-micro dispersive solidphase extraction
Mineral, pond, and
wastewater
Ultrahigh-performance liquid
chromatography-tandem
mass spectrometry;
Column: C18
(50 mm
 2.1 mm, 1.7μm)
Recovery:70–120%;
LODs:0.002–0.06μg/L;
RSDs:<20%
Santana-Mayor
et al. (2018)
6
Magnetic molecularly imprinted
polymer solid-phase extraction
Lake, river, and tap
water
Gas chromatography–tandem
mass spectrometry;
Column:HP-5MS
(30 m
 250 mm, 0.25 mm)
Recovery:86.1–103.1%;
LODs:0.0016–0.0052
μg/
L;
RSDs:<6.7%
Yang et al. (2016)
4
Solid-phase microextraction
Bottled mineral
water
Gas chromatography-flame
ionization detection;
Column: CP-SIL 8CB
(25 m
 0.32 mm, 0.25
μm)
Recovery:86–107%;
LOD:0.05–0.12
μg/L;
RSD:6.6–11.1%
Banitaba et al.
(2013)
564
C. Sun et al.