5
Solid-phase extraction
Tap and bottled
water
High-performance liquid
chromatography-ultraviolet
detection;
Column: C18
(150 mm
 4.6 mm,5
μm)
Recovery:84.3–105.5%;
LODs:0.09–0.33μg/L;
RSDs:0.3–7.6%
Luo et al. (2014)
15
Dispersive solid-phase
microextraction
Ultrapure water,
river, and seawater
Gas chromatography–mass
spectrometry;
Column:HP-5MS
(30 m
 0.25 mm., 0.25μm)
Recovery 71–117%;:
LODs:2–7μg/L;
RSDs:1–10%
Wu et al. (2013)
6
Magnetic solid-phase extraction
Bottled water
Gas chromatography–tandem
mass spectrometry;
Column:DB-5MS
(60 m
 0.32 mm, 1μm)
Recovery:87.5–99.1%;
LOD:0.005–0.01μg/L;
RSD:0.6–7.7%
Pinsrithong and
Bunkoed (2018)
7
Magnetic solid-phase extraction
Water
High-performance liquid
chromatography-ultraviolet
detection;
Column: C18
(250 mm
 4.6 mm, 5
μm)
Recovery: 77–120%;
LODs:0.02–0.05μg/L;
RSDs:1.0–4.9% (intraday)
Wang et al.
(2019a)
5
Molecularly imprinted polymersolid-phase microextraction
Reservoir water, tap
water, and bottled
water
Gas chromatography–tandem
mass spectrometry;
Column: DB-17
(30 m
 0.25 mm,0.25
μm)
Recovery:94.54–105.34%;
LODs:0.02–0.34μg/L;
RSDs:1.5–8.04%
He et al. (2010)
8
Molecularly imprinted polymersolid-phase extraction
River, lake, pond,
and wellwater
Gas chromatography–tandem
mass spectrometry;
Column: HP-5MS
(30 m
 250 mm,0.25 mm)
Recovery:>92.9%;
LODs:0.01–0.05μg/L;
RSDs:<3.8%
Guo et al. (2019)
(continued)
15 Analytical Methods for Phthalates in Water Samples
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