Table 4
(continued)
Pharmaceuticals
MAE extraction conditions
Clean-up
Analysis
References
Soil
mass
(g)
Solvent (power
in watt)
Time
(min)
 number
of cycles
Temp
(
C)
Recovery
(%)
RSD
(%)
LOD
Instrument
Sulfaguanidine,
sulfacetamide, sulfadiazine,
sulfathiazole, sulfapyridine,
sulfamethazine,
sulfamerazine, sulfamethoxazole, and
sulfadimethoxine
1 g
Methanol
45 min
 1
110
C
Sub- to low
ng per g
LC-MS/MS
[99]
Tetracycline,
deoxytetracycline, oxytetracycline, chlortetracycline
1 g
Methanol
(400 W)
20 min
60
C
μ-SPE device
consisted of copper
(II) isonicotinate
70.6–
110.5%
<15.1% 0.1–6.3 ng/
g
HPLC-UV
[100]
440
R. Manasfi et al.