30
4 Experimental Data
1.2d N-Isopropyl-4-methylbenzenesulfonamide
The product was prepared from 381 mg (2 mmol) 4-methylbenzenesulfonyl chloride and 355 mg (6 mmol) iso-propylamine in 95% (404 mg) yield according to
the general procedure B. All spectroscopic properties are in good accordance with
reported data.
[45]
1.2e N-Benzyl-4-methylbenzenesulfonamide
The product was prepared from 381 mg (2 mmol) 4-methylbenzenesulfonyl chloride and 643 mg (6 mmol) benzylamine in 94% (489 mg) yield according to the
general procedure B. All spectroscopic properties are in good accordance with reported data.
[46]
1.2f 4-Methyl-N-phenylbenzenesulfonamide
The product was prepared from 381 mg (2 mmol) 4-methylbenzenesulfonyl chloride and 559 mg (6 mmol) aniline in 87% (432 mg) yield according to the general
procedure B. All spectroscopic properties are in good accordance with reported
data.
[46]
4 Experimental Data
1.2d N-Isopropyl-4-methylbenzenesulfonamide
The product was prepared from 381 mg (2 mmol) 4-methylbenzenesulfonyl chloride and 355 mg (6 mmol) iso-propylamine in 95% (404 mg) yield according to
the general procedure B. All spectroscopic properties are in good accordance with
reported data.
[45]
1.2e N-Benzyl-4-methylbenzenesulfonamide
The product was prepared from 381 mg (2 mmol) 4-methylbenzenesulfonyl chloride and 643 mg (6 mmol) benzylamine in 94% (489 mg) yield according to the
general procedure B. All spectroscopic properties are in good accordance with reported data.
[46]
1.2f 4-Methyl-N-phenylbenzenesulfonamide
The product was prepared from 381 mg (2 mmol) 4-methylbenzenesulfonyl chloride and 559 mg (6 mmol) aniline in 87% (432 mg) yield according to the general
procedure B. All spectroscopic properties are in good accordance with reported
data.
[46]