Table 2.5 Detection Limits Comparison (pg pf PANH per Injection on LC Column).
Dibenz Dibenz
Methyl
Methyl
Methyl
Benzo[h] Phenan Phenan
Benz [c] [a,j]
[c,h]
Method
Quinoline Phthalazine Quinazoline quinoline quinoline quinoline Acridine quinoline throline thorline Benz[a] acridine acridine acridine
a
LC/MS/MS
7.9 2.6
15
0.8
4.4
2.6
1.0
0.4
0.9
0.3
0.5
0.7
0.6
1.6
b
LC/MS/MS
24
42
18
15
12
22
74
56
69
11
38
25
29
32
b
LC/DAD
2140
4000
2290
5080
2080
2100
1130
1110
5000
2260
943
1170
973
950
b
LC/FLD
12700
No FL.
3970
1520
2980
1040
7.4
39
69
25
7.6
6.0
2.1
111
Notes.
a
3
× S/N method
b
Graham method
Reprinted from Svabensky et al, International Journal of Environmental Analytical Chemistry 2009, 89 167, © 2009 Taylor and Frances [202].