108
7 Hybrid Technologies in Action: Sonochemistry and Beyond
Table 7.1 a
NH
2 –H
2 BDC
2-aminoterephthalic acid; b
SBET is the BET specific surface area; c
Micropore volume is the total specific pore volume determined
using the adsorption branch of the N
2 isotherm at P/P
0
0.99
Sample name
Molar ratio
NH
2 –H
2 BDC a
:Al(NO
3 )
3 :DMF
Time
Yield (%)
SBET/(m 2
g −1
) b
Micropore volume/(cm
3
g −1
) c
a
4.5:3:30
10 min
68
499
1.03
b
4.5:3:30
15 min
84
529
2.10
c
4.5:3:30
20 min
91
568
3.78
d
4.5:3:30
25 min
95
636
3.53
Hydrothermal
4.5:3:30
72 h
90
1036
3.0
7 Hybrid Technologies in Action: Sonochemistry and Beyond
Table 7.1 a
NH
2 –H
2 BDC
2-aminoterephthalic acid; b
SBET is the BET specific surface area; c
Micropore volume is the total specific pore volume determined
using the adsorption branch of the N
2 isotherm at P/P
0
0.99
Sample name
Molar ratio
NH
2 –H
2 BDC a
:Al(NO
3 )
3 :DMF
Time
Yield (%)
SBET/(m 2
g −1
) b
Micropore volume/(cm
3
g −1
) c
a
4.5:3:30
10 min
68
499
1.03
b
4.5:3:30
15 min
84
529
2.10
c
4.5:3:30
20 min
91
568
3.78
d
4.5:3:30
25 min
95
636
3.53
Hydrothermal
4.5:3:30
72 h
90
1036
3.0