9
Head-space solid-phase
microextraction
Bottled water
Gas chromatography–mass
spectrometry;
Column: DB-5MS
(30 m
 0.25 mm, 0.25
μm,
LODs:0.003–0.085μg/L;
RSDs:0.78–21.7%
Cao (2008)
3
Online solid-phase extraction
Bottled water
High-performance liquid
chromatography-ultraviolet
detection;
Column: C18
(250 mm
 4.6 mm, 5
μm)
Recovery:80–115%;
LOD:0.7–2.4μg/L;
RSD:0.9–4.0%
Salazar-Beltrán
et al. (2017)
5
Solid-phase microextraction
Water
Gas chromatography-flame
ionization detection;
Column: HP-5
(30 m
 0.32 mm, 0.25μm)
LOD:0.003–10
μg/L;
RSD:2.16–19%
Li et al. (2006)
16
Solid-phase microextraction
Seawater
Gas chromatography–mass
spectrometry;
Column: DB-1MS (30 m
Â
0.25 mm, 0.25
μm)
Recovery:55.4–114%;
LODs:0.005–0.32μg/L;
RSDs:0.24–8.8%
Zhang et al.
(2017)
9
Hollow
fiber-based liquid–liquid
microextraction
Mineral, pond, tap,
and wastewater
Gas chromatography–tandem
mass spectrometry;
Column: SPB-5
(30 m
 0.25 mm, 0.25
μm)
Recovery: 74–120%;
RSDs:<20%
González-Sálamo
et al. (2018)
5
Magnetic solid-phase extraction
River water
High-performance liquid
chromatography-ultraviolet
detection,
Column: ZORBAX SB-C18
(150 mm
 4.6 mm, 5μm)
Recovery:92.4–104.7%;
LODs:0.025–0.089μg/L;
RSDs:<6%
Wang et al.
(2019a, b, c)
(continued)
15 Analytical Methods for Phthalates in Water Samples
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