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66. Jodłowski PJ, Jędrzejczyk RJ, Chlebda D, Gierda M, Łojewska J (2017) In situ
spectroscopic studies of methane catalytic combustion over Co, Ce, and Pd mixed oxides
deposited on a steel surface. J Catal 350:1–12
67. Becker E, Carlsson P, Kylhammar L, Newton MA, Skoglundh M (2011) In situ
spectroscopic investigation of low-temperature oxidation of methane over
alumina-supported platinum during periodic operation. J Phys Chem C 115:944–951
68. Rutkowska M, Díaz U, Palomares AE, Chmielarz L (2015) Cu and Fe modified derivatives
of 2D MWW-type zeolites (MCM-22, ITQ-2 and MCM-36) as new catalysts for DeNO x
process. Appl Catal B Environ 168–169:531–539
69. Chlebda DK, Jodłowski PJ, Jędrzejczyk RJ, Łojewska J (2018) Generalised two-dimensional
correlation analysis of the Co, Ce, and Pd mixed oxide catalytic systems for methane
combustion using in situ infrared spectroscopy. Spectrochim Acta, Part A 192:202–210
70. Chlebda DK, Jodłowski PJ, Jędrzejczyk RJ, Łojewska J (2017) 2D-COS of in situ l-Raman
and in situ IR spectra for structure evolution characterisation of NEP-deposited cobalt oxide
catalyst during n-nonane combustion. Spectrochim Acta, Part A 186:44–51
71. Marinkovic NS, Wang Q, Barrio L, Ehrlich SN, Khalid S, Cooper C, Frenkel AI (2011)
Combined in situ X-ray absorption and diffuse reflectance infrared spectroscopy: An
attractive tool for catalytic investigations. Nucl Instruments Methods Phys Res Sect A Accel
Spectrometers, Detect Assoc Equip 649:204–206
72. Brieger C, Melke J, Van der Bosch N, Reinholz U, Riesemeier H, Guilherme Buzanich A,
Kayarkatte MK, Derr I, Schökel A, Roth C (2016) A combined in-situ XAS-DRIFTS study
unraveling adsorbate induced changes on the Pt nanoparticle structure. J Catal 339:57–67
73. Parlett CMA, Gaskell CV, Naughton JN, Newton MA, Wilson K, Lee AF (2013) Operando
synchronous DRIFTS/MS/XAS as a powerful tool for guiding the design of Pd catalysts for
the selective oxidation of alcohols. Catal Today 205:76–85
74. Jodłowski PJ, Chlebda D, Piwowarczyk E, Chrzan M, Jędrzejczyk RJ, Sitarz M,
Węgrzynowicz A, Kołodziej A, Łojewska J (2016) In situ and operando spectroscopic
studies of sonically aided catalysts for biogas exhaust abatement. J Mol Struct 1126:132–140
75. Zaera F (2014) New advances in the use of infrared absorption spectroscopy for the
characterization of heterogeneous catalytic reactions. Chem Soc Rev 43:7624–7663
76. Iwamoto M, Hoshino Y (1995) Time-resolved FT-IR study on isotopic exchange of ditrosyl
species strongly adsorbed on Co-MFI zeolite. Chem Lett 24:729–730
77. Yeom YH, Frei H (2003) Step-scan FT-IR monitoring of transient HCO radicals in a room
temperature zeolite. J Phys Chem B 107:6286–6291
78. Zhang M, De Respinis M, Frei H (2014) Time-resolved observations of water oxidation
intermediates on a cobalt oxide nanoparticle catalyst. Nat Chem 6:362–367
79. Chang BK, Jang BW, Dai S, Overbury SH (2005) Transient studies of the mechanisms of
CO oxidation over Au/TiO 2 using time-resolved FTIR spectroscopy and product analysis.
J Catal 236:392–400
80. Chen T, Feng Z, Wu G, Shi J, Ma G, Ying P, Li C (2007) Mechanistic studies of
photocatalytic reaction of methanol for hydrogen production on Pt/TiO 2 by in situ fourier
transform IR and time-resolved IR spectroscopy. J Phys Chem C 111:8005–8014
81. Yao S, Mudiyanselage K, Xu W, Johnston-Peck AC, Hanson JC, Wu T, Stacchiola D,
Rodriguez JA, Zhao H, Beyer KA, Chapman KW, Chupas PJ, Martínez-Arias A, Si R,
Bolin TB, Liu W, Senanayake SD (2014) Unraveling the dynamic nature of a CuO/CeO 2
catalyst for CO oxidation in Operando: a combined study of XANES (fluorescence) and
drifts. ACS Catal 4:1650–1661
82. Kang M, Perry D, Kim YR, Colburn AW, Lazenby RA, Unwin PR (2015) Time-resolved
detection and analysis of single nanoparticle electrocatalytic impacts. J Am Chem Soc
137:10902–10905
11 In Situ and Operando Techniques in Catalyst Characterisation …
357
different length and time scales. Angew Chemie Int Ed 48:4910–4943
66. Jodłowski PJ, Jędrzejczyk RJ, Chlebda D, Gierda M, Łojewska J (2017) In situ
spectroscopic studies of methane catalytic combustion over Co, Ce, and Pd mixed oxides
deposited on a steel surface. J Catal 350:1–12
67. Becker E, Carlsson P, Kylhammar L, Newton MA, Skoglundh M (2011) In situ
spectroscopic investigation of low-temperature oxidation of methane over
alumina-supported platinum during periodic operation. J Phys Chem C 115:944–951
68. Rutkowska M, Díaz U, Palomares AE, Chmielarz L (2015) Cu and Fe modified derivatives
of 2D MWW-type zeolites (MCM-22, ITQ-2 and MCM-36) as new catalysts for DeNO x
process. Appl Catal B Environ 168–169:531–539
69. Chlebda DK, Jodłowski PJ, Jędrzejczyk RJ, Łojewska J (2018) Generalised two-dimensional
correlation analysis of the Co, Ce, and Pd mixed oxide catalytic systems for methane
combustion using in situ infrared spectroscopy. Spectrochim Acta, Part A 192:202–210
70. Chlebda DK, Jodłowski PJ, Jędrzejczyk RJ, Łojewska J (2017) 2D-COS of in situ l-Raman
and in situ IR spectra for structure evolution characterisation of NEP-deposited cobalt oxide
catalyst during n-nonane combustion. Spectrochim Acta, Part A 186:44–51
71. Marinkovic NS, Wang Q, Barrio L, Ehrlich SN, Khalid S, Cooper C, Frenkel AI (2011)
Combined in situ X-ray absorption and diffuse reflectance infrared spectroscopy: An
attractive tool for catalytic investigations. Nucl Instruments Methods Phys Res Sect A Accel
Spectrometers, Detect Assoc Equip 649:204–206
72. Brieger C, Melke J, Van der Bosch N, Reinholz U, Riesemeier H, Guilherme Buzanich A,
Kayarkatte MK, Derr I, Schökel A, Roth C (2016) A combined in-situ XAS-DRIFTS study
unraveling adsorbate induced changes on the Pt nanoparticle structure. J Catal 339:57–67
73. Parlett CMA, Gaskell CV, Naughton JN, Newton MA, Wilson K, Lee AF (2013) Operando
synchronous DRIFTS/MS/XAS as a powerful tool for guiding the design of Pd catalysts for
the selective oxidation of alcohols. Catal Today 205:76–85
74. Jodłowski PJ, Chlebda D, Piwowarczyk E, Chrzan M, Jędrzejczyk RJ, Sitarz M,
Węgrzynowicz A, Kołodziej A, Łojewska J (2016) In situ and operando spectroscopic
studies of sonically aided catalysts for biogas exhaust abatement. J Mol Struct 1126:132–140
75. Zaera F (2014) New advances in the use of infrared absorption spectroscopy for the
characterization of heterogeneous catalytic reactions. Chem Soc Rev 43:7624–7663
76. Iwamoto M, Hoshino Y (1995) Time-resolved FT-IR study on isotopic exchange of ditrosyl
species strongly adsorbed on Co-MFI zeolite. Chem Lett 24:729–730
77. Yeom YH, Frei H (2003) Step-scan FT-IR monitoring of transient HCO radicals in a room
temperature zeolite. J Phys Chem B 107:6286–6291
78. Zhang M, De Respinis M, Frei H (2014) Time-resolved observations of water oxidation
intermediates on a cobalt oxide nanoparticle catalyst. Nat Chem 6:362–367
79. Chang BK, Jang BW, Dai S, Overbury SH (2005) Transient studies of the mechanisms of
CO oxidation over Au/TiO 2 using time-resolved FTIR spectroscopy and product analysis.
J Catal 236:392–400
80. Chen T, Feng Z, Wu G, Shi J, Ma G, Ying P, Li C (2007) Mechanistic studies of
photocatalytic reaction of methanol for hydrogen production on Pt/TiO 2 by in situ fourier
transform IR and time-resolved IR spectroscopy. J Phys Chem C 111:8005–8014
81. Yao S, Mudiyanselage K, Xu W, Johnston-Peck AC, Hanson JC, Wu T, Stacchiola D,
Rodriguez JA, Zhao H, Beyer KA, Chapman KW, Chupas PJ, Martínez-Arias A, Si R,
Bolin TB, Liu W, Senanayake SD (2014) Unraveling the dynamic nature of a CuO/CeO 2
catalyst for CO oxidation in Operando: a combined study of XANES (fluorescence) and
drifts. ACS Catal 4:1650–1661
82. Kang M, Perry D, Kim YR, Colburn AW, Lazenby RA, Unwin PR (2015) Time-resolved
detection and analysis of single nanoparticle electrocatalytic impacts. J Am Chem Soc
137:10902–10905
11 In Situ and Operando Techniques in Catalyst Characterisation …
357