44. Kung MC, Lin SSY, Kung HH (2012) In situ infrared spectroscopic study of CH 4 oxidation
over Co-ZSM-5. Top Catal 55:108–115
45. Ferri D, Bürgi T, Baiker A (2001) Pt and Pt/Al2O3 thin films for investigation of catalytic
solid-liquid interfaces by ATR-IR spectroscopy: CO adsorption, H2-induced reconstruction
and surface-enhanced absorption. J Phys Chem B 105:3187–3195
46. Ferri D, Bürgi T, Baiker A (2002) Probing boundary sites on a Pt/Al 2 O 3 model catalyst by
CO 2 hydrogenation and in situ ATR-IR spectroscopy of catalytic solid–liquid interfaces.
Phys Chem Chem Phys 4:2667–2672
47. Burgener M, Wirz R, Mallat T, Baiker A (2004) Nature of catalyst deactivation during citral
hydrogenation: a catalytic and ATR-IR study. J Catal 228:152–161
48. Grabow K, Bentrup U (2014) Homogeneous catalytic processes monitored by combined
in situ. ACS Catal 4:2153–2164
49. Rabeah J, Bentrup U, StoBer R, Bruckner A (2015) Selective alcohol oxidation by a copper
TEMPO catalyst: mechanistic insights by simultaneously coupled operando EPR/UV-Vis/
ATR-IR spectroscopy. Angew Chemie Int Ed 54:11791–11794
50. Ohlin L, Bazin P, Thibault-Starzyk F, Hedlund J, Mattias Grahn M (2013) Adsorption of
CO 2 , CH 4 , and H 2 O in zeolite ZSM-5 studied using in situ ATR-FTIR spectroscopy. J Phys
Chem C 117:16972–16982
51. Savara A, Weitz E (2014) Elucidation of intermediates and mechanisms in heterogeneous
catalysis using infrared spectroscopy. Annu Rev Phys Chem 65:249–273
52. Xu Z, Yu J, Jaroniec M (2015) Efficient catalytic removal of formaldehyde at room
temperature using AlOOH nanoflakes with deposited Pt. Appl Catal B Environ 163:306–312
53. Macina D, Piwowarska Z, Góra-Marek K, Tarach K, Rutkowska M, Girman V,
Blachowski A, Chmielarz L (2016) SBA-15 loaded with iron by various methods as
catalyst for DeNO x process. Mater Res Bull 78:72–82
54. Murakami N, Koga N (2016) In situ photoacoustic FTIR studies on photocatalytic oxidation
of 2-propanol over titanium(IV) oxide. Catal Commun 83:1–4
55. Qi L, Cheng B, Yu J, Ho W (2016) High-surface area mesoporous Pt/TiO 2 hollow chains for
efficient formaldehyde decomposition at ambient temperature. Elsevier BV
56. Haw JF (2002) In-situ spectroscopy in heterogeneous catalysis. Wiley-VCH
57. Rasmussen SB, Portela R, Bazin P, Ávila P, Banares MA, Daturi M (2018) Transient
operando study on the NH 3 /NH 4
+ interplay in V-SCR monolithic catalysts. Appl Catal B
Environ 224:109–115
58. Thibault-Starzyk F, Mauge F (2012) Infrared Spectroscopy. In: Che M, Védrine J
(eds) Characterization of solid materials and heterogeneous catalysts. From structure to
surface reactivity. Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim, pp 3–48
59. Benaliouche F, Boucheffa Y, Thibault-Starzyk F (2012) In situ FTIR studies of propene
adsorption over Ag- and Cu-exchanged Y zeolites. Microporous Mesoporous Mater 147:10–
16
60. El-Roz M, Bazin P, Daturi M, Thibault-Starzyk F (2013) Operando IR coupled to SSITKA
for photocatalysis: reactivity and mechanistic studies. ACS Catal 3:2790–2798
61. El-Roz M, Kus M, Cool P, Thibault-Starzyk F (2012) New operando IR technique to study
the photocatalytic activity and selectivity of TiO 2 nanotubes in air purification: Influence of
temperature, UV intensity, and VOC concentration. J Phys Chem C 116:13252–13263
62. Keturakis CJ, Zhu M, Gibson EK, Daturi M, Tao F, Frenkel AI, Wachs IE (2016) Dynamics
of CrO 3 –Fe 2 O 3 catalysts during the high-temperature water-gas shift reaction: molecular
structures and reactivity. ACS Catal 6:4786–4798
63. Mitchell MB (1993) Fundamentals and applications of diffuse reflectance infrared fourier
transform (DRIFT) spectroscopy. In: Urban MW, Craver CD (eds) Structure-property
relations in polymers, spectroscopy and performance. American Chemical Society,
Washington, DC, pp 351–375
64. Hamadeh IM, King D, Griffiths PR (1984) Heatable-evacuable cell and optical system for
diffuse reflectance FT-IR spectrometry of adsorbed species. J Catal 88:264–272
356
P. Jodłowski and J. Łojewska
over Co-ZSM-5. Top Catal 55:108–115
45. Ferri D, Bürgi T, Baiker A (2001) Pt and Pt/Al2O3 thin films for investigation of catalytic
solid-liquid interfaces by ATR-IR spectroscopy: CO adsorption, H2-induced reconstruction
and surface-enhanced absorption. J Phys Chem B 105:3187–3195
46. Ferri D, Bürgi T, Baiker A (2002) Probing boundary sites on a Pt/Al 2 O 3 model catalyst by
CO 2 hydrogenation and in situ ATR-IR spectroscopy of catalytic solid–liquid interfaces.
Phys Chem Chem Phys 4:2667–2672
47. Burgener M, Wirz R, Mallat T, Baiker A (2004) Nature of catalyst deactivation during citral
hydrogenation: a catalytic and ATR-IR study. J Catal 228:152–161
48. Grabow K, Bentrup U (2014) Homogeneous catalytic processes monitored by combined
in situ. ACS Catal 4:2153–2164
49. Rabeah J, Bentrup U, StoBer R, Bruckner A (2015) Selective alcohol oxidation by a copper
TEMPO catalyst: mechanistic insights by simultaneously coupled operando EPR/UV-Vis/
ATR-IR spectroscopy. Angew Chemie Int Ed 54:11791–11794
50. Ohlin L, Bazin P, Thibault-Starzyk F, Hedlund J, Mattias Grahn M (2013) Adsorption of
CO 2 , CH 4 , and H 2 O in zeolite ZSM-5 studied using in situ ATR-FTIR spectroscopy. J Phys
Chem C 117:16972–16982
51. Savara A, Weitz E (2014) Elucidation of intermediates and mechanisms in heterogeneous
catalysis using infrared spectroscopy. Annu Rev Phys Chem 65:249–273
52. Xu Z, Yu J, Jaroniec M (2015) Efficient catalytic removal of formaldehyde at room
temperature using AlOOH nanoflakes with deposited Pt. Appl Catal B Environ 163:306–312
53. Macina D, Piwowarska Z, Góra-Marek K, Tarach K, Rutkowska M, Girman V,
Blachowski A, Chmielarz L (2016) SBA-15 loaded with iron by various methods as
catalyst for DeNO x process. Mater Res Bull 78:72–82
54. Murakami N, Koga N (2016) In situ photoacoustic FTIR studies on photocatalytic oxidation
of 2-propanol over titanium(IV) oxide. Catal Commun 83:1–4
55. Qi L, Cheng B, Yu J, Ho W (2016) High-surface area mesoporous Pt/TiO 2 hollow chains for
efficient formaldehyde decomposition at ambient temperature. Elsevier BV
56. Haw JF (2002) In-situ spectroscopy in heterogeneous catalysis. Wiley-VCH
57. Rasmussen SB, Portela R, Bazin P, Ávila P, Banares MA, Daturi M (2018) Transient
operando study on the NH 3 /NH 4
+ interplay in V-SCR monolithic catalysts. Appl Catal B
Environ 224:109–115
58. Thibault-Starzyk F, Mauge F (2012) Infrared Spectroscopy. In: Che M, Védrine J
(eds) Characterization of solid materials and heterogeneous catalysts. From structure to
surface reactivity. Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim, pp 3–48
59. Benaliouche F, Boucheffa Y, Thibault-Starzyk F (2012) In situ FTIR studies of propene
adsorption over Ag- and Cu-exchanged Y zeolites. Microporous Mesoporous Mater 147:10–
16
60. El-Roz M, Bazin P, Daturi M, Thibault-Starzyk F (2013) Operando IR coupled to SSITKA
for photocatalysis: reactivity and mechanistic studies. ACS Catal 3:2790–2798
61. El-Roz M, Kus M, Cool P, Thibault-Starzyk F (2012) New operando IR technique to study
the photocatalytic activity and selectivity of TiO 2 nanotubes in air purification: Influence of
temperature, UV intensity, and VOC concentration. J Phys Chem C 116:13252–13263
62. Keturakis CJ, Zhu M, Gibson EK, Daturi M, Tao F, Frenkel AI, Wachs IE (2016) Dynamics
of CrO 3 –Fe 2 O 3 catalysts during the high-temperature water-gas shift reaction: molecular
structures and reactivity. ACS Catal 6:4786–4798
63. Mitchell MB (1993) Fundamentals and applications of diffuse reflectance infrared fourier
transform (DRIFT) spectroscopy. In: Urban MW, Craver CD (eds) Structure-property
relations in polymers, spectroscopy and performance. American Chemical Society,
Washington, DC, pp 351–375
64. Hamadeh IM, King D, Griffiths PR (1984) Heatable-evacuable cell and optical system for
diffuse reflectance FT-IR spectrometry of adsorbed species. J Catal 88:264–272
356
P. Jodłowski and J. Łojewska