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gas chromatographic column and identification by time of flight mass spectrometry. Lipids
48:1279–1295. https://doi.org/10.1007/s11745-013-3830-2
60. Dettmer K (2014) Assessment of ionic liquid stationary phases for the GC analysis of fatty
acid methyl esters. Anal Bioanal Chem 406:4931–4939. https://doi.org/10.1007/s00216-0147919-0
61. Mjøs SA (2003) Identification of fatty acids in gas chromatography by application of different
temperature and pressure programs on a single capillary column. J Chromatogr A 1015:151–
161. https://doi.org/10.1016/S0021-9673(03)01240-8
62. Mjøs SA, Grahl-Nielsen O (2006) Prediction of gas chromatographic retention of polyunsaturated fatty acid methyl esters. J Chromatogr A 1110:171–180. https://doi.org/10.1016/j.
chroma.2006.01.092
63. Pinto AC, Guarieiro LLN, Rezende MJC, Ribeiro NM, Torres EA, Lopes WA, de P Pereira
PA, de Andrade JB (2005) Biodiesel: an overview. J Braz Chem Soc 16:1313–1330. http://
dx.doi.org/10.1590/S0103-50532005000800003
64. Webster RL, Rawson PM, Evans DJ, Marriott PJ (2016) Quantification of trace fatty acid
methyl esters in diesel fuel by using multidimensional gas chromatography with electron and
chemical ionization mass spectrometry. J Sep Sci 39:2537–2543. https://doi.org/10.1002/jssc.
201600307
65. Ragonese C, Tranchida PQ, Sciarrone D, Mondello L (2009) Conventional and fast gas chromatography analysis of biodiesel blends using an ionic liquid stationary phase. J Chromatogr
A 1216:8992–8997. https://doi.org/10.1016/j.chroma.2009.10.066
66. Goding JC, Ragon DY, O’Connor JB, Boehm SJ, Hupp AM (2013) Comparison of GC stationary phases for the separation of fatty acid methyl esters in biodiesel fuels. Anal Bioanal
Chem 405:6087–6094. https://doi.org/10.1007/s00216-013-7042-7
67. Mogollon NGS, de Lima Ribeiro FA, Lopez MM, Hantao LW, Poppi RJ, Augusto F (2013)
Quantitative analysis of biodiesel in blends of biodiesel and conventional diesel by comprehensive two-dimensional gas chromatography and multivariate curve resolution. Anal Chim
Acta 796:130–136. https://doi.org/10.1016/j.aca.2013.07.071
68. Takahashi Sato R, Stroppa PHF, da Silva AD, de Oliveira MAL (2016) Fast GC-FID method
for monitoring acidic and basic catalytic transesterification reactions in vegetable oils to
methyl ester biodiesel preparation. Quim Nova 39:352–355. http://dx.doi.org/10.5935/01004042.20160027
69. Mogollón NGS, Ribeiro FAL, Poppi RJ, Quintana AL, Chávez JAG, Agualongo DAP, Aleme
HG, Augusto F (2017) Exploratory analysis of biodiesel by combining comprehensive twodimensional gas chromatography and multiway principal component analysis. J Braz Chem
Soc 28:740–746. http://dx.doi.org/10.21577/0103-5053.20160222
70. Webster RL, Evans DJ, Marriott PJ (2015) Detailed chemical analysis using multidimensional
gas chromatography–mass spectrometry and bulk properties of low-temperature oxidized jet
fuels. Energy Fuels 29:2059–2066. https://doi.org/10.1021/acs.energyfuels.5b00264
71. McCormick RL, Graboski MS, Alleman TL, Herring AM, Tyson KS (2001) Impact of
biodiesel source material and chemical structure on emissions of criteria pollutants from
a heavy-duty engine. Environ Sci Technol 35:1742–1747. https://doi.org/10.1021/es001636t
72. Sushchik NN, Kuchkina AYu, Gladyshev MI (2013) Fatty acid content and composition of
sediments from Siberian eutrophic water bodies: Implications for biodiesel production. Water
Res 47:3192–3200. https://doi.org/10.1016/j.watres.2013.03.031
73. Knothe G, Sharp CA, Ryan III TW (2006) Exhaust emissions of biodiesel, petrodiesel, neat
methyl esters, and alkanes in a new technology engine. Energy Fuels 20:403–408. https://
doi.org/10.1021/ef0502711
74. CSN EN 14331 (2004) Liquid petroleum products - Separation and characterization of
fatty acid methyl esters (FAME) from middle distillates - Liquid chromatography (LC)/gas
chromatography (GC). European Committee for Standardization, Brussels
75. Katona G, Andréasson U, Landau EM, Andréasson L-E, Neutze R (2003) Lipidic cubic phase
crystal structure of the photosynthetic reaction centre from Rhodobacter sphaeroides at 2.35 Å
resolution. J Mol Biol 331:681–692. https://doi.org/10.1016/S0022-2836(03)00751-4
M. Talebi et al.
gas chromatographic column and identification by time of flight mass spectrometry. Lipids
48:1279–1295. https://doi.org/10.1007/s11745-013-3830-2
60. Dettmer K (2014) Assessment of ionic liquid stationary phases for the GC analysis of fatty
acid methyl esters. Anal Bioanal Chem 406:4931–4939. https://doi.org/10.1007/s00216-0147919-0
61. Mjøs SA (2003) Identification of fatty acids in gas chromatography by application of different
temperature and pressure programs on a single capillary column. J Chromatogr A 1015:151–
161. https://doi.org/10.1016/S0021-9673(03)01240-8
62. Mjøs SA, Grahl-Nielsen O (2006) Prediction of gas chromatographic retention of polyunsaturated fatty acid methyl esters. J Chromatogr A 1110:171–180. https://doi.org/10.1016/j.
chroma.2006.01.092
63. Pinto AC, Guarieiro LLN, Rezende MJC, Ribeiro NM, Torres EA, Lopes WA, de P Pereira
PA, de Andrade JB (2005) Biodiesel: an overview. J Braz Chem Soc 16:1313–1330. http://
dx.doi.org/10.1590/S0103-50532005000800003
64. Webster RL, Rawson PM, Evans DJ, Marriott PJ (2016) Quantification of trace fatty acid
methyl esters in diesel fuel by using multidimensional gas chromatography with electron and
chemical ionization mass spectrometry. J Sep Sci 39:2537–2543. https://doi.org/10.1002/jssc.
201600307
65. Ragonese C, Tranchida PQ, Sciarrone D, Mondello L (2009) Conventional and fast gas chromatography analysis of biodiesel blends using an ionic liquid stationary phase. J Chromatogr
A 1216:8992–8997. https://doi.org/10.1016/j.chroma.2009.10.066
66. Goding JC, Ragon DY, O’Connor JB, Boehm SJ, Hupp AM (2013) Comparison of GC stationary phases for the separation of fatty acid methyl esters in biodiesel fuels. Anal Bioanal
Chem 405:6087–6094. https://doi.org/10.1007/s00216-013-7042-7
67. Mogollon NGS, de Lima Ribeiro FA, Lopez MM, Hantao LW, Poppi RJ, Augusto F (2013)
Quantitative analysis of biodiesel in blends of biodiesel and conventional diesel by comprehensive two-dimensional gas chromatography and multivariate curve resolution. Anal Chim
Acta 796:130–136. https://doi.org/10.1016/j.aca.2013.07.071
68. Takahashi Sato R, Stroppa PHF, da Silva AD, de Oliveira MAL (2016) Fast GC-FID method
for monitoring acidic and basic catalytic transesterification reactions in vegetable oils to
methyl ester biodiesel preparation. Quim Nova 39:352–355. http://dx.doi.org/10.5935/01004042.20160027
69. Mogollón NGS, Ribeiro FAL, Poppi RJ, Quintana AL, Chávez JAG, Agualongo DAP, Aleme
HG, Augusto F (2017) Exploratory analysis of biodiesel by combining comprehensive twodimensional gas chromatography and multiway principal component analysis. J Braz Chem
Soc 28:740–746. http://dx.doi.org/10.21577/0103-5053.20160222
70. Webster RL, Evans DJ, Marriott PJ (2015) Detailed chemical analysis using multidimensional
gas chromatography–mass spectrometry and bulk properties of low-temperature oxidized jet
fuels. Energy Fuels 29:2059–2066. https://doi.org/10.1021/acs.energyfuels.5b00264
71. McCormick RL, Graboski MS, Alleman TL, Herring AM, Tyson KS (2001) Impact of
biodiesel source material and chemical structure on emissions of criteria pollutants from
a heavy-duty engine. Environ Sci Technol 35:1742–1747. https://doi.org/10.1021/es001636t
72. Sushchik NN, Kuchkina AYu, Gladyshev MI (2013) Fatty acid content and composition of
sediments from Siberian eutrophic water bodies: Implications for biodiesel production. Water
Res 47:3192–3200. https://doi.org/10.1016/j.watres.2013.03.031
73. Knothe G, Sharp CA, Ryan III TW (2006) Exhaust emissions of biodiesel, petrodiesel, neat
methyl esters, and alkanes in a new technology engine. Energy Fuels 20:403–408. https://
doi.org/10.1021/ef0502711
74. CSN EN 14331 (2004) Liquid petroleum products - Separation and characterization of
fatty acid methyl esters (FAME) from middle distillates - Liquid chromatography (LC)/gas
chromatography (GC). European Committee for Standardization, Brussels
75. Katona G, Andréasson U, Landau EM, Andréasson L-E, Neutze R (2003) Lipidic cubic phase
crystal structure of the photosynthetic reaction centre from Rhodobacter sphaeroides at 2.35 Å
resolution. J Mol Biol 331:681–692. https://doi.org/10.1016/S0022-2836(03)00751-4