Table 6
(continued)
Matrix and target
molecules
Weight/
volume of
sample
Extraction solvent
Salts
Buffer
Clean-up
Analytical
method
Reference
4 macrolides, and
lincomycin
MeOH:phosphoric
acid 5% (7:1:2, v/v)
Lettuce
– lincomycin,
roxithromycin, doxycycline hyclate,
demeclocycline, sulfamethoxazole,
oxytetracycline
2 g wet
weight
10 mL (80% isopropyl alcohol, 20%
0,04 M citric acid
solution)
None (freezethaw extraction)
None
SPE clean-up
(200 mg Oasis
HLB)
LC-MS/MS
[166]
Brassica juncea
–
acetaminophen
0,5 g wet
weight
(root and
leaf)
1 mL HCl 0,1 M
None (solidliquid
extraction)
None
SPE method,
Phenomenex StrataX 300 mg
LC-MS
[28]
Cucumber, eggplant, long
bean, and wheat
–
sulfamonomethoxine,
sulfathiazole, acetylsulfamethoxazole,
sulfisoxazole,
sulfachlorpyridazine,
sulfamethazine,
sulfamerazine, trimethoprim, chloramphenicol,
ibuprofen, sulfamethoxazole, and triclosan
5 g wet
grain crop
2 g wet
fruit and
vegetables
220 mL ACN
None (Soxhlet
extraction)
None
None
LC-MS/MS
QqQ
[34]
462
R. Manasfi et al.
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