Table 6
(continued)
Matrix and target
molecules
Weight/
volume of
sample
Extraction solvent
Salts
Buffer
Clean-up
Analytical
method
Reference
Cabbage
– salbutamol, trimethoprim, sulfamethoxazole, carbamazepine,
sertraline, triclosan
8 g wet
plant
50 mL ACN:H
2 O
(55:45, v/v)
None (pressurized liquid
extraction, PLE)
None
None
LC-MS
[40]
Carrot, potato
–
bezafibrate, carbamazepine, diclofenac, gemfibrozil, ibuprofen, clofibric
acid, sulfapyridine,
ketoprofen, sulfamethoxazole, 10,11epoxycarbamazepine
1 g dry
weight
MeOH +1 g Florisil None (ASE
method)
None
None
LC-MS
[125]
Lettuce and carrot
– tetracycline and amoxicillin
0,1 g dry
weight
100% Milli-Q water
(final extract 30 mL)
None (PLE
method)
None
SPE clean-up (Oasis
HLB cartridges
hydrophiliclipophilic balance,
200 mg/6 mL)
LC-MS/MS
QTrap Sciex
[39]
Grass
– oxytetracycline,
sulfamethoxazole,
ketoconazole
1 g wet
weight
MeOH:citric acid
(0,2 M, 50:50, v/v,
pH
¼ 4,5 with
NaOH)
None (PLE
method)
Na
2 EDTA
SPE clean-up
(Strata-X 200 mg/
6 mL, reverse phase)
LC-MS
Orbitrap
Thermo
Fisher
[165]
Soybean and wheat
–
ketoprofen, naproxen,
diclofenac, ibuprofen
0,5 g dry
weight
0,01 M NaOH
None (pressurized hot water
extraction
–
ASE)
None
Hollow
fiber liquidphase
microextraction
clean-up
LC-MS
[131]
460
R. Manasfi et al.