Lettuce crops
– 24 carbamazepine transformation
products
10 g wet
weight
10 mL of MeCN at
1% of acetic acid
6 g of MgSO
4
1.5 g of NaOAc
d-SPE (125 mg
PSA, 125 mg C18,
750 mg anhydrous
MgSO
4 )
LC-QTOFMS/MS
[155]
Lepidium sativum
– atorvastatin,
fluvastatin,
simvastatin
1 g wet
weight
4 mL ACN:H
2 O
(1:1, v/v)
1.2 g MgSO
4 ,
0.3 g NaCl
None
None
HPLC DTIM
QTOF-MS,
HPLC
QQQ/MS/
MS
[156]
Soil and beet root
–
bisoprolol, metoprolol, sulfamethoxazole, trimethoprim, caffeine
10 g dry
weight
10 mL ACN (1%
acetic acid)
4 g anhydrous
MgSO
4 , 1 g
NaCl
1 g trisodium citrate dehydrate,
0.5 g disodium
hydrogen citrate
sesquihydrate
150 mg PSA,
900 MgSO
4 mg,
150 mg C18
LC-MS/MS
[157]
Lettuce, maize, and radish
– atenolol, carbamazepine, and triclosan
1 g dry
weight
10 mL ACN
4 g MgSO
4 + 1 g
NaCl
Bond Elut
QuEChERS Dispersive Universal
Kit
None
LC-MS/MS
QqQ
[158]
Chicory
– diclofenac
2 g wet
weight
4 mL ACN
2 g
MgSO
4 + 0,5 g
NaCl
0,5 g sodium citrate tribasic
dihydrate +0,25 g
sodium citrate
dibasic
sesquihydrate
150 mg
MgSO
4 + 25 mg
PSA + 25 mg C18E
UPLC-MS/
MS QToF
[159]
Lettuce
–
4-hydroxydiclofenac,
5-methyl-benzotriazole,
acesulfame, acetaminophen, acridone,
benzotriazole, bezafibrate,
1 g dry
weight
10 mL CAN +50
μL
formic acid
4 g MgSO
4 + 1 g
NaCl
None
150 mg PSA,
900 MgSO
4 mg,
150 mg C18
HPLC-MS/
MS QToF
[160]
(continued)
Development of Methods for the Determination of PhACs in Soil/Earthworm/Crop. . .
455