112
6 Particulate Silica Reinforcement of Rubber
Fig. 6.4 TEM image of
particulate silica generated
in situ in the peroxide
cross-linked IR (from Fig. 1
in Ref. [55])
nanoparticles of silica are dispersed well in the cross-linked IR. Figure 6.5 shows the
time-resolved two-dimensional small-angle X-ray scattering (2D-SAXS) patterns
under uniaxial elongation (100 mm/min) measured using synchrotron radiation at
Stretching direction
Elongation ratio
Stress (MPa)
Stretching direction
Fig. 6.5 Two-dimensional SAXS patterns and speculated morphological change of the in situ
silica-filled IR nanocomposite during tensile deformation (modified Fig. 3 in Ref. [55], and from
Fig. 4 in Ref. [34])
6 Particulate Silica Reinforcement of Rubber
Fig. 6.4 TEM image of
particulate silica generated
in situ in the peroxide
cross-linked IR (from Fig. 1
in Ref. [55])
nanoparticles of silica are dispersed well in the cross-linked IR. Figure 6.5 shows the
time-resolved two-dimensional small-angle X-ray scattering (2D-SAXS) patterns
under uniaxial elongation (100 mm/min) measured using synchrotron radiation at
Stretching direction
Elongation ratio
Stress (MPa)
Stretching direction
Fig. 6.5 Two-dimensional SAXS patterns and speculated morphological change of the in situ
silica-filled IR nanocomposite during tensile deformation (modified Fig. 3 in Ref. [55], and from
Fig. 4 in Ref. [34])