50. Parrilla Vazquez P, Mughari AR, Galera MM (2008) Solid-phase microextraction (SPME) for
the determination of pyrethroids in cucumber and watermelon using liquid chromatography
combined with post-column photochemically induced fluorimetry derivatization and fluorescence detection. Anal Chem Acta 607:74–82
51. Goulart SM, de Queiroz MELR, Neves AA, de Queiroz JH (2008) Low-temperature clean-up
method for the determination of pyrethroids in milk using gas chromatography with electron
capture detection. Talanta 75:1320–1323
52. Li B, Zheng F, Dong Q, Cao Y, Fan H, Deng C (2012) Rapid determination method for
12 pyrethroid pesticide residues in tea by stir bar sorptive extraction-thermal desorption-gas
chromatography. Phys Procedia 25:1776–1780
53. Khalili Zanjani MR, Yamini Y, Shariati S, Jönsson JÅ (2007) A new liquid-phase
microextraction method based on solidification of floating organic drop. Anal Chim Acta
585:286–293
54. Arthur CL, Pawliszyn J (1990) Solid phase microextraction with thermal desorption using fused
silica optical fibers. Anal Chem 62:2145–2148
55. Pawliszyn J (1997) Solid phase microextraction. In: Theory and practice. Wiley, New York
56. You J, Weston DP, Lydy MJ (2004) A sonication extraction method for the analysis of
pyrethroid, organophosphate, and organochlorine pesticides from sediment by gas chromatography with electron-capture detection. Arch Environ Contam Toxicol 47:141–147
57. Anastassiades M, Lehotay SJ, Stajnbaher D, Schenck FJ (2003) Fast and easy multiresidue
method employing acetonitrile extraction/partitioning and “dispersive solid-phase extraction”
for the determination of pesticide residues in produce. J AOAC Int 86:412–413
58. Maguire RJ (1990) Chemical and photochemical isomerization of deltamethrin. J Agric Food
Chem 38:1613–1617
59. Audino PG, de Licastro SA, Zerba E (1999) Thermal behaviour and biological activity of
pyrethroids in smoke-generating formulations. Pestic Sci 55:1187–1193
60. Ruzo LO, Holmstead RL, Casida JE (1977) Pyrethroid photochemistry: decamethrin. J Agric
Food Chem 25:1385–1394
61. Valverde A, Aguilera A, Rodriguez M, Boulaid M (2002) What are we determining using gas
chromatographic multiresidue methods: tralomethrin or deltamethrin? J Chromatogr A
943:101–111
62. Liu W, Qin S, Gan J (2005) Chiral stability of synthetic pyrethroid insecticides. J Agric Food
Chem 53:3814–3820
63. Godula M, Hajšlová J, Alterová K (1999) Pulsed splitless injection and the extent of matrix
effects in the analysis of pesticides. J High Resolut Chromatogr 22:395–402
64. Wylie PL (1996) Improved gas chromatographic analysis of organophosphorus pesticides with
pulsed splitless injection. J AOAC Int 79:571–577
65. Feo ML, Eljarrat E, Barcelò D (2011) Performance of mass chromatography/tandem mass
spectrometry in the analysis of pyrethroid insecticides in environmental and food samples.
Rapid Comm Mass Spectrom 25:869–876
66. Lòpez-Lòpez T, Gil Garcìa MD, Martínez Vidal JL, Martínez M (2001) Determination of
pyrethroids in vegetables by HPLC using continuous on-line post-elution photoirradiation with
fluorescence detection. Anal Chim Acta 447:101–111
67. Olsson AO, Baker SE, Nguyen JV, Romanoff LC, Ununka SO, Walter RD, Flemmen KL,
Barr DB (2004) A liquid chromatographyÀtandem mass spectrometry multiresidue method for
quantification of specific metabolites of organophosphorus pesticides, synthetic pyrethroids,
selected herbicides, and DEET in human urine. Anal Chem 76:2453–2461
68. Aaron JJ (1993) Schulman SG (ed) Molecular luminescence spectrometry: methods and
applications. Wiley, New York, p 85
69. Liu WP, Gan JJ (2004) Separation and analysis of diastereomers and enantiomers of
cypermethrin and cyfluthrin by gas chromatography. J Agric Food Chem 52:755–761
44
M. L. Feo
the determination of pyrethroids in cucumber and watermelon using liquid chromatography
combined with post-column photochemically induced fluorimetry derivatization and fluorescence detection. Anal Chem Acta 607:74–82
51. Goulart SM, de Queiroz MELR, Neves AA, de Queiroz JH (2008) Low-temperature clean-up
method for the determination of pyrethroids in milk using gas chromatography with electron
capture detection. Talanta 75:1320–1323
52. Li B, Zheng F, Dong Q, Cao Y, Fan H, Deng C (2012) Rapid determination method for
12 pyrethroid pesticide residues in tea by stir bar sorptive extraction-thermal desorption-gas
chromatography. Phys Procedia 25:1776–1780
53. Khalili Zanjani MR, Yamini Y, Shariati S, Jönsson JÅ (2007) A new liquid-phase
microextraction method based on solidification of floating organic drop. Anal Chim Acta
585:286–293
54. Arthur CL, Pawliszyn J (1990) Solid phase microextraction with thermal desorption using fused
silica optical fibers. Anal Chem 62:2145–2148
55. Pawliszyn J (1997) Solid phase microextraction. In: Theory and practice. Wiley, New York
56. You J, Weston DP, Lydy MJ (2004) A sonication extraction method for the analysis of
pyrethroid, organophosphate, and organochlorine pesticides from sediment by gas chromatography with electron-capture detection. Arch Environ Contam Toxicol 47:141–147
57. Anastassiades M, Lehotay SJ, Stajnbaher D, Schenck FJ (2003) Fast and easy multiresidue
method employing acetonitrile extraction/partitioning and “dispersive solid-phase extraction”
for the determination of pesticide residues in produce. J AOAC Int 86:412–413
58. Maguire RJ (1990) Chemical and photochemical isomerization of deltamethrin. J Agric Food
Chem 38:1613–1617
59. Audino PG, de Licastro SA, Zerba E (1999) Thermal behaviour and biological activity of
pyrethroids in smoke-generating formulations. Pestic Sci 55:1187–1193
60. Ruzo LO, Holmstead RL, Casida JE (1977) Pyrethroid photochemistry: decamethrin. J Agric
Food Chem 25:1385–1394
61. Valverde A, Aguilera A, Rodriguez M, Boulaid M (2002) What are we determining using gas
chromatographic multiresidue methods: tralomethrin or deltamethrin? J Chromatogr A
943:101–111
62. Liu W, Qin S, Gan J (2005) Chiral stability of synthetic pyrethroid insecticides. J Agric Food
Chem 53:3814–3820
63. Godula M, Hajšlová J, Alterová K (1999) Pulsed splitless injection and the extent of matrix
effects in the analysis of pesticides. J High Resolut Chromatogr 22:395–402
64. Wylie PL (1996) Improved gas chromatographic analysis of organophosphorus pesticides with
pulsed splitless injection. J AOAC Int 79:571–577
65. Feo ML, Eljarrat E, Barcelò D (2011) Performance of mass chromatography/tandem mass
spectrometry in the analysis of pyrethroid insecticides in environmental and food samples.
Rapid Comm Mass Spectrom 25:869–876
66. Lòpez-Lòpez T, Gil Garcìa MD, Martínez Vidal JL, Martínez M (2001) Determination of
pyrethroids in vegetables by HPLC using continuous on-line post-elution photoirradiation with
fluorescence detection. Anal Chim Acta 447:101–111
67. Olsson AO, Baker SE, Nguyen JV, Romanoff LC, Ununka SO, Walter RD, Flemmen KL,
Barr DB (2004) A liquid chromatographyÀtandem mass spectrometry multiresidue method for
quantification of specific metabolites of organophosphorus pesticides, synthetic pyrethroids,
selected herbicides, and DEET in human urine. Anal Chem 76:2453–2461
68. Aaron JJ (1993) Schulman SG (ed) Molecular luminescence spectrometry: methods and
applications. Wiley, New York, p 85
69. Liu WP, Gan JJ (2004) Separation and analysis of diastereomers and enantiomers of
cypermethrin and cyfluthrin by gas chromatography. J Agric Food Chem 52:755–761
44
M. L. Feo