Table 2
(continued)
Analytes
Matrix
Sample
preparation
Instrumental
analysis
MLODs
Recovery (%)
Ref.
DELT
Rat tissue (liver,
brain, kidney)
Mix and centrifugation
with organic
solvent
HPLC-UV-Vis
0.1
μg mL
À1
95–114 for liver, 97–108 for
kidney, 95–108 for brain
[40]
CYPE, DELT
Porcine tissue
(liver, heart, muscle, and kidney)
MSPD
HPLC-UV
Not reported
95.6–90.5–85.8 and 97.8 for
CYPE and 92.3, 86.2, 103.8,
and 104.1 for DELT in the
liver, muscle, heart, and kidney, respectively
[41]
DELT, CYPE
Fish tissue
QuEChERS
GC-MS
0.3 ng/g
35–135
[42]
TETR, FENP, CYHA, CYPE,
FENV, DELT
Fish
QuEChERS
modified
Fluorescence
spectrophotometer
0.008–0.014
μg/mL 76–89
[43]
TETR, PHEN, CYHA, PERM,
CYFL, FENP, DELT
Blood
SPE
GC-HRMS
17–93 pg/mL
37–84
[44]
Food samples
FENP, DELT, PERM, BIFE
Honey
IL-DMME
HPLC-VWD
(variable wavelength detector)
0.03–0.05
μg/L
87–92
[45]
FENP, CYHA, PERM, DELT Oil vegetable
DLLME
GC-FID
0.02–0.16 mg/kg
85–109
[46]
TETR, FENP, CYPE, DELT,
FENV, PERM
Fruit juice
DLLME
HPLC-UV
2–5
μg/L
84–94
[47]
CYPE, PERM
Wine, fruit, and
vegetables
ELISA
GC-MS
5–10
μg/kg
74–99
[48]
TRAN, ALLE, BIFE, CYHA,
PERM, CYFL, CYPE, FENV,
DELT
Rice
QuEChERS
GC-MS-MS
1
μg/kg
87–117
[49]
28
M. L. Feo