324
for reaction monitoring and in situ yield determinations for an early stage pharmaceutical
candidate. Anal Chem 83:8766–8771
9. Pauli GF, Gödecke T, Jaki BU et al (2012)
Quantitative
1
H NMR: development and
potential of an analytical method: an update. J
Nat Prod 75:834–851
10. Schneider H-J, Hacket F, Volker R (1988)
NMR studies of cyclodextrins and cyclodextrin
complexes. Chem Rev 98:1755–1785
11. Dugoni GC, Pietro M, Ferro M et al (2019)
Effect of water on DES/β-cyclodextrin systems. ACS Sustain Chem Eng 7:7277–7285
12. Inoue Y, Shinohara I, Murata I et al (2019)
Study on the molecular stability, solubility, and
diffusibility of guaiazulene included in β- and
γ-cyclodextrin. J Mol Struct 1186:50–59
13. Leyva E, Moctezuma E, Strouse J et al (2001)
Spectrometric and 2D NMR studies on the
complexation of chlorophenols with cyclodextrins. J Incl Phenom 39:41–46
14. Bendeby B, Kenne L, Sandström C (2004)
1
H-NMR studies of the inclusion complexes
between α-cyclodextrin and adamantane derivatives using both exchangeable hydroxy protons and non-exchangeable aliphatic protons.
J Incl Phenom Macrocycl Chem 50:173–181
15. Hakkarainen B, Fujita K, Immel S et al (2005)
1
H-NMR studies on the hydrogen-bonding
network in mono-altro-β-cyclodextrin and its
complex with adamantane-1-carboxylic acid.
Carbohydr Res 340(8):1539–1545
16. Wójcik J, Ejchart A, Nowakowski M (2019)
Shape adaptation of quinine in cyclodextrin
cavities: NMR studies. Phys Chem Chem Phys
21:6925–6934
17. Fielding L (2000) Determination of association constants (K a ) from solution NMR data.
Tetrahedron 56:6151–6170
18. Monticelli C, Fantin G, Carmine G et al (2019)
Inclusion of 5-mercapto-1-phenyl-tetrazole
into β-cyclodextrin for entrapment in silane
Fig. 5
13
C MAS NMR spectra of five samples recorded at 45 °C
Dimitrios Ntountaniotis et al.
for reaction monitoring and in situ yield determinations for an early stage pharmaceutical
candidate. Anal Chem 83:8766–8771
9. Pauli GF, Gödecke T, Jaki BU et al (2012)
Quantitative
1
H NMR: development and
potential of an analytical method: an update. J
Nat Prod 75:834–851
10. Schneider H-J, Hacket F, Volker R (1988)
NMR studies of cyclodextrins and cyclodextrin
complexes. Chem Rev 98:1755–1785
11. Dugoni GC, Pietro M, Ferro M et al (2019)
Effect of water on DES/β-cyclodextrin systems. ACS Sustain Chem Eng 7:7277–7285
12. Inoue Y, Shinohara I, Murata I et al (2019)
Study on the molecular stability, solubility, and
diffusibility of guaiazulene included in β- and
γ-cyclodextrin. J Mol Struct 1186:50–59
13. Leyva E, Moctezuma E, Strouse J et al (2001)
Spectrometric and 2D NMR studies on the
complexation of chlorophenols with cyclodextrins. J Incl Phenom 39:41–46
14. Bendeby B, Kenne L, Sandström C (2004)
1
H-NMR studies of the inclusion complexes
between α-cyclodextrin and adamantane derivatives using both exchangeable hydroxy protons and non-exchangeable aliphatic protons.
J Incl Phenom Macrocycl Chem 50:173–181
15. Hakkarainen B, Fujita K, Immel S et al (2005)
1
H-NMR studies on the hydrogen-bonding
network in mono-altro-β-cyclodextrin and its
complex with adamantane-1-carboxylic acid.
Carbohydr Res 340(8):1539–1545
16. Wójcik J, Ejchart A, Nowakowski M (2019)
Shape adaptation of quinine in cyclodextrin
cavities: NMR studies. Phys Chem Chem Phys
21:6925–6934
17. Fielding L (2000) Determination of association constants (K a ) from solution NMR data.
Tetrahedron 56:6151–6170
18. Monticelli C, Fantin G, Carmine G et al (2019)
Inclusion of 5-mercapto-1-phenyl-tetrazole
into β-cyclodextrin for entrapment in silane
Fig. 5
13
C MAS NMR spectra of five samples recorded at 45 °C
Dimitrios Ntountaniotis et al.