USEFUL SYNTHETIC PREPARATIONS
VI.A.6-14 Rao, P.N. et al., CC, 1985.
351
Me
F 2 , CaO, THF, MeOH
Me
Me
I
N, H
90%
VLA.6-15 Nelson, W.L. et al., JMC, 37, 2856; Bhattacharyya, S., TL, 35,
2401; Fujii, T. et al., CPB, 42, 383; Montanari, V. and Resnati, G., TL, 35,
8015.
NH 2
Me
Ar
v>
1: Et0 2 CH
NH
N.
2: BH 3 DMS, THF
Ar
,Ν.
81 %
VLA.6-16 Dell, C.P. et al., H, 38, 399; Guram, A.S. and Buchwald, S.L.,
JACS, 116, 7901; Yasuda, M. et al., BCJ, 67, 246.
CN
0 2 N
R 2 NH, EtOH
CN
60-85 %
VLA.6-17 Banwell, M.G. et al., CC, 61.
Br
Br
l:AgNCO,A
2: (-)-menthol
NHC0 2 R
Br 94 %
R = mentholyl