1 3
Topics in Current Chemistry (2020) 378:40
86. Joseyphus RJ, Kodama D, Matsumoto T, Sato Y, Jeyadevan B, Tohji K (2007) Role of polyol in the
synthesis of Fe particles. J Magn Magn Mater 310(2 Part 3):2393–2395. https ://doi.org/10.1016/j.
jmmm.2006.10.1132
87. Cheng C, Xu F, Gu H (2011) Facile synthesis and morphology evolution of magnetic iron oxide
nanoparticles in different polyol processes. New J Chem 35(5):1072–1079. https ://doi.org/10.1039/
C0NJ0 0986E
88. Hachani R, Lowdell M, Birchall M, Hervault A, Mertz D, Begin-Colin S, Thanh NTK (2016) Polyol synthesis, functionalisation, and biocompatibility studies of superparamagnetic iron oxide nanoparticles as potential MRI contrast agents. Nanoscale 8(6):3278–3287. https ://doi.org/10.1039/
C5NR0 3867G
89. Gavilán H, Sánchez EH, Brollo MEF, Asín L, Moerner KK, Frandsen C, Lázaro FJ, Serna CJ,
Veintemillas-Verdaguer S, Morales MP, Gutiérrez L (2017) Formation mechanism of maghemite
nanoflowers synthesized by a polyol-mediated process. ACS Omega 2(10):7172–7184. https ://doi.
org/10.1021/acsom ega.7b009 75
90. Hu F, MacRenaris KW, Waters EA, Liang T, Schultz-Sikma EA, Eckermann AL, Meade TJ (2009)
Ultrasmall, water-soluble magnetite nanoparticles with high relaxivity for magnetic resonance
imaging. J Phys Chem C 113(49):20855–20860. https ://doi.org/10.1021/jp907 216g
91. Wan J, Cai W, Meng X, Liu E (2007) Monodisperse water-soluble magnetite nanoparticles prepared by polyol process for high-performance magnetic resonance imaging. Chem Commun
47:5004–5006. https ://doi.org/10.1039/B7127 95B
92. Cai W, Wan J (2007) Facile synthesis of superparamagnetic magnetite nanoparticles in liquid polyols. J Colloid Interface Sci 305(2):366–370. https ://doi.org/10.1016/j.jcis.2006.10.023
93. Hemery G, Keyes AC, Garaio E, Rodrigo I, Garcia JA, Plazaola F, Garanger E, Sandre O (2017)
Tuning sizes, morphologies, and magnetic properties of monocore versus multicore iron oxide
nanoparticles through the controlled addition of water in the polyol synthesis. Inorg Chem
56(14):8232–8243. https ://doi.org/10.1021/acs.inorg chem.7b009 56
94. Wetegrove M, Witte K, Bodnar W, Pfahl D-E, Springer A, Schell N, Westphal F, Burkel E (2019)
Formation of maghemite nanostructures in polyol: tuning the particle size via the precursor stoichiometry. CrystEngComm 21(12):1956–1966. https ://doi.org/10.1039/C8CE0 2115E
95. Maity D, Chandrasekharan P, Si-Shen F, Xue J-M, Ding J (2010) Polyol-based synthesis of hydrophilic magnetite nanoparticles. J Appl Phys 107(9):09B310. https ://doi.org/10.1063/1.33558 98
96. Qu H, Ma H, Riviere A, Zhou W, O’Connor CJ (2012) One-pot synthesis in polyamines for preparation of water-soluble magnetite nanoparticles with amine surface reactivity. J Mater Chem
22(8):3311–3313. https ://doi.org/10.1039/C2JM1 5932E
97. Wang J, Zhang B, Wang L, Wang M, Gao F (2015) One-pot synthesis of water-soluble superparamagnetic iron oxide nanoparticles and their MRI contrast effects in the mouse brains. Mater Sci
Eng, C 48:416–423. https ://doi.org/10.1016/j.msec.2014.12.026
98. Kandasamy G, Soni S, Sushmita K, Veerapu NS, Bose S, Maity D (2019) One-step synthesis of
hydrophilic functionalized and cytocompatible superparamagnetic iron oxide nanoparticles (SPIONs) based aqueous ferrofluids for biomedical applications. J Mol Liq 274:653–663. https ://doi.
org/10.1016/j.molli q.2018.10.161
99. Miao C, Hu F, Rui Y, Duan Y, Gu H (2019) A T1/T2 dual functional iron oxide MRI contrast agent
with super stability and low hypersensitivity benefited by ultrahigh carboxyl group density. J Mater
Chem B 7(12):2081–2091. https ://doi.org/10.1039/C9TB0 0002J
100. Babić-Stojić B, Jokanović V, Milivojević D, Požek M, Jagličić Z, Makovec D, Orsini NJ, Marković
M, Arsikin K, Paunović V (2018) Ultrasmall iron oxide nanoparticles: magnetic and NMR relaxometric properties. Curr Appl Phys 18(2):141–149. https ://doi.org/10.1016/j.cap.2017.11.017
101. Yoo D, Lee C, Seo B, Piao Y (2017) One pot synthesis of amine-functionalized and angular-shaped superparamagnetic iron oxide nanoparticles for MR/fluorescence bimodal imaging
application. RSC Adv 7(21):12876–12885. https ://doi.org/10.1039/C6RA2 8495G
102. Wagle DV, Rondinone AJ, Woodward JD, Baker GA (2017) Polyol synthesis of magnetite
nanocrystals in a thermostable ionic liquid. Cryst Growth Des 17(4):1558–1567. https ://doi.
org/10.1021/acs.cgd.6b015 11
103. Durães L, Costa BFO, Vasques J, Campos J, Portugal A (2005) Phase investigation of as-prepared iron oxide/hydroxide produced by sol–gel synthesis. Mater Lett 59(7):859–863. https ://
doi.org/10.1016/j.matle t.2004.10.066
79
Reprinted from the journal
Topics in Current Chemistry (2020) 378:40
86. Joseyphus RJ, Kodama D, Matsumoto T, Sato Y, Jeyadevan B, Tohji K (2007) Role of polyol in the
synthesis of Fe particles. J Magn Magn Mater 310(2 Part 3):2393–2395. https ://doi.org/10.1016/j.
jmmm.2006.10.1132
87. Cheng C, Xu F, Gu H (2011) Facile synthesis and morphology evolution of magnetic iron oxide
nanoparticles in different polyol processes. New J Chem 35(5):1072–1079. https ://doi.org/10.1039/
C0NJ0 0986E
88. Hachani R, Lowdell M, Birchall M, Hervault A, Mertz D, Begin-Colin S, Thanh NTK (2016) Polyol synthesis, functionalisation, and biocompatibility studies of superparamagnetic iron oxide nanoparticles as potential MRI contrast agents. Nanoscale 8(6):3278–3287. https ://doi.org/10.1039/
C5NR0 3867G
89. Gavilán H, Sánchez EH, Brollo MEF, Asín L, Moerner KK, Frandsen C, Lázaro FJ, Serna CJ,
Veintemillas-Verdaguer S, Morales MP, Gutiérrez L (2017) Formation mechanism of maghemite
nanoflowers synthesized by a polyol-mediated process. ACS Omega 2(10):7172–7184. https ://doi.
org/10.1021/acsom ega.7b009 75
90. Hu F, MacRenaris KW, Waters EA, Liang T, Schultz-Sikma EA, Eckermann AL, Meade TJ (2009)
Ultrasmall, water-soluble magnetite nanoparticles with high relaxivity for magnetic resonance
imaging. J Phys Chem C 113(49):20855–20860. https ://doi.org/10.1021/jp907 216g
91. Wan J, Cai W, Meng X, Liu E (2007) Monodisperse water-soluble magnetite nanoparticles prepared by polyol process for high-performance magnetic resonance imaging. Chem Commun
47:5004–5006. https ://doi.org/10.1039/B7127 95B
92. Cai W, Wan J (2007) Facile synthesis of superparamagnetic magnetite nanoparticles in liquid polyols. J Colloid Interface Sci 305(2):366–370. https ://doi.org/10.1016/j.jcis.2006.10.023
93. Hemery G, Keyes AC, Garaio E, Rodrigo I, Garcia JA, Plazaola F, Garanger E, Sandre O (2017)
Tuning sizes, morphologies, and magnetic properties of monocore versus multicore iron oxide
nanoparticles through the controlled addition of water in the polyol synthesis. Inorg Chem
56(14):8232–8243. https ://doi.org/10.1021/acs.inorg chem.7b009 56
94. Wetegrove M, Witte K, Bodnar W, Pfahl D-E, Springer A, Schell N, Westphal F, Burkel E (2019)
Formation of maghemite nanostructures in polyol: tuning the particle size via the precursor stoichiometry. CrystEngComm 21(12):1956–1966. https ://doi.org/10.1039/C8CE0 2115E
95. Maity D, Chandrasekharan P, Si-Shen F, Xue J-M, Ding J (2010) Polyol-based synthesis of hydrophilic magnetite nanoparticles. J Appl Phys 107(9):09B310. https ://doi.org/10.1063/1.33558 98
96. Qu H, Ma H, Riviere A, Zhou W, O’Connor CJ (2012) One-pot synthesis in polyamines for preparation of water-soluble magnetite nanoparticles with amine surface reactivity. J Mater Chem
22(8):3311–3313. https ://doi.org/10.1039/C2JM1 5932E
97. Wang J, Zhang B, Wang L, Wang M, Gao F (2015) One-pot synthesis of water-soluble superparamagnetic iron oxide nanoparticles and their MRI contrast effects in the mouse brains. Mater Sci
Eng, C 48:416–423. https ://doi.org/10.1016/j.msec.2014.12.026
98. Kandasamy G, Soni S, Sushmita K, Veerapu NS, Bose S, Maity D (2019) One-step synthesis of
hydrophilic functionalized and cytocompatible superparamagnetic iron oxide nanoparticles (SPIONs) based aqueous ferrofluids for biomedical applications. J Mol Liq 274:653–663. https ://doi.
org/10.1016/j.molli q.2018.10.161
99. Miao C, Hu F, Rui Y, Duan Y, Gu H (2019) A T1/T2 dual functional iron oxide MRI contrast agent
with super stability and low hypersensitivity benefited by ultrahigh carboxyl group density. J Mater
Chem B 7(12):2081–2091. https ://doi.org/10.1039/C9TB0 0002J
100. Babić-Stojić B, Jokanović V, Milivojević D, Požek M, Jagličić Z, Makovec D, Orsini NJ, Marković
M, Arsikin K, Paunović V (2018) Ultrasmall iron oxide nanoparticles: magnetic and NMR relaxometric properties. Curr Appl Phys 18(2):141–149. https ://doi.org/10.1016/j.cap.2017.11.017
101. Yoo D, Lee C, Seo B, Piao Y (2017) One pot synthesis of amine-functionalized and angular-shaped superparamagnetic iron oxide nanoparticles for MR/fluorescence bimodal imaging
application. RSC Adv 7(21):12876–12885. https ://doi.org/10.1039/C6RA2 8495G
102. Wagle DV, Rondinone AJ, Woodward JD, Baker GA (2017) Polyol synthesis of magnetite
nanocrystals in a thermostable ionic liquid. Cryst Growth Des 17(4):1558–1567. https ://doi.
org/10.1021/acs.cgd.6b015 11
103. Durães L, Costa BFO, Vasques J, Campos J, Portugal A (2005) Phase investigation of as-prepared iron oxide/hydroxide produced by sol–gel synthesis. Mater Lett 59(7):859–863. https ://
doi.org/10.1016/j.matle t.2004.10.066
79
Reprinted from the journal