1 3
Topics in Current Chemistry (2020) 378:40
48. Roca AG, Morales MP, Serna CJ (2006) Synthesis of monodispersed magnetite particles from different organometallic precursors. IEEE Trans Magn 42(10):3025–3029. https ://doi.org/10.1109/
TMAG.2006.88011 1
49. Guardia P, Riedinger A, Nitti S, Pugliese G, Marras S, Genovese A, Materia ME, Lefevre C,
Manna L, Pellegrino T (2014) One pot synthesis of monodisperse water soluble iron oxide
nanocrystals with high values of the specific absorption rate. J Mater Chem B 2(28):4426–4434.
https ://doi.org/10.1039/C4TB0 0061G
50. Kim BH, Lee N, Kim H, An K, Park YI, Choi Y, Shin K, Lee Y, Kwon SG, Na HB, Park J-G,
Ahn T-Y, Kim Y-W, Moon WK, Choi SH, Hyeon T (2011) Large-scale synthesis of uniform and
extremely small-sized iron oxide nanoparticles for high-resolution T1 magnetic resonance imaging
contrast agents. J Am Chem Soc 133(32):12624–12631. https ://doi.org/10.1021/ja203 340u
51. Kovalenko MV, Bodnarchuk MI, Lechner RT, Hesser G, Schäffler F, Heiss W (2007) Fatty acid
salts as stabilizers in size- and shape-controlled nanocrystal synthesis: the case of inverse spinel
iron oxide. J Am Chem Soc 129(20):6352–6353. https ://doi.org/10.1021/ja069 2478
52. Mourdikoudis S, Liz-Marzán LM (2013) Oleylamine in nanoparticle synthesis. Chem Mater
25(9):1465–1476. https ://doi.org/10.1021/cm400 0476
53. Hou Y, Xu Z, Sun S (2007) Controlled synthesis and chemical conversions of FeO nanoparticles.
Angew Chem Int Ed 46(33):6329–6332. https ://doi.org/10.1002/anie.20070 1694
54. Nemati Z, Alonso J, Rodrigo I, Das R, Garaio E, García JÁ, Orue I, Phan M-H, Srikanth H (2018)
Improving the heating efficiency of iron oxide nanoparticles by tuning their shape and size. J Phys
Chem C 122(4):2367–2381. https ://doi.org/10.1021/acs.jpcc.7b105 28
55. Park J, Lee E, Hwang N-M, Kang M, Kim SC, Hwang Y, Park J-G, Noh H-J, Kim J-Y, Park J-H,
Hyeon T (2005) One-nanometer-scale size-controlled synthesis of monodisperse magnetic iron
oxide nanoparticles. Angew Chem Int Ed 44(19):2872–2877. https ://doi.org/10.1002/anie.20046
1665
56. Li Z, Sun Q, Gao M (2005) Preparation of water-soluble magnetite nanocrystals from hydrated ferric salts in 2-pyrrolidone: mechanism leading to Fe 3 O 4 . Angew Chem Int Ed 44(1):123–126. https
://doi.org/10.1002/anie.20046 0715
57. Xu Z, Shen C, Hou Y, Gao H, Sun S (2009) Oleylamine as both reducing agent and stabilizer in a
facile synthesis of magnetite nanoparticles. Chem Mater 21(9):1778–1780. https ://doi.org/10.1021/
cm802 978z
58. Yang H, Ogawa T, Hasegawa D, Takahashi M (2008) Synthesis and magnetic properties of monodisperse magnetite nanocubes. J Appl Phys 103(7):07D526. https ://doi.org/10.1063/1.28338 20
59. Mohapatra J, Mitra A, Bahadur D, Aslam M (2013) Surface controlled synthesis of MFe 2 O 4
(M = Mn, Fe Co, Ni and Zn) nanoparticles and their magnetic characteristics. CrystEngComm
15(3):524–532. https ://doi.org/10.1039/C2CE2 5957E
60. Macdonald JE, Brooks CJ, Veinot JGC (2008) The influence of trace water concentration on iron
oxide nanoparticle size. Chem Commun 32:3777–3779. https ://doi.org/10.1039/B8057 15J
61. Unni M, Uhl AM, Savliwala S, Savitzky BH, Dhavalikar R, Garraud N, Arnold DP, Kourkoutis LF,
Andrew JS, Rinaldi C (2017) Thermal decomposition synthesis of iron oxide nanoparticles with
diminished magnetic dead layer by controlled addition of oxygen. ACS Nano 11(2):2284–2303.
https ://doi.org/10.1021/acsna no.7b006 09
62. Li Z, Chen H, Bao H, Gao M (2004) One-pot reaction to synthesize water-soluble magnetite
nanocrystals. Chem Mater 16(8):1391–1393. https ://doi.org/10.1021/cm035 346y
63. Ooi F, DuChene JS, Qiu J, Graham JO, Engelhard MH, Cao G, Gai Z, Wei WD (2015) A facile
solvothermal synthesis of octahedral Fe 3 O 4 nanoparticles. Small 11(22):2649–2653. https ://doi.
org/10.1002/smll.20140 1954
64. Bunge A, Porav AS, Borodi G, Radu T, Pîrnău A, Berghian-Grosan C, Turcu R (2019) Correlation
between synthesis parameters and properties of magnetite clusters prepared by solvothermal polyol
method. J Mater Sci 54(4):2853–2875. https ://doi.org/10.1007/s1085 3-018-3030-9
65. Mao B, Kang Z, Wang E, Lian S, Gao L, Tian C, Wang C (2006) Synthesis of magnetite octahedrons from iron powders through a mild hydrothermal method. Mater Res Bull 41(12):2226–2231.
https ://doi.org/10.1016/j.mater resbu ll.2006.04.037
66. Giri J, Guha Thakurta S, Bellare J, Kumar Nigam A, Bahadur D (2005) Preparation and characterization of phospholipid stabilized uniform sized magnetite nanoparticles. J Magn Magn Mater
293(1):62–68. https ://doi.org/10.1016/j.jmmm.2005.01.044
77
Reprinted from the journal
Topics in Current Chemistry (2020) 378:40
48. Roca AG, Morales MP, Serna CJ (2006) Synthesis of monodispersed magnetite particles from different organometallic precursors. IEEE Trans Magn 42(10):3025–3029. https ://doi.org/10.1109/
TMAG.2006.88011 1
49. Guardia P, Riedinger A, Nitti S, Pugliese G, Marras S, Genovese A, Materia ME, Lefevre C,
Manna L, Pellegrino T (2014) One pot synthesis of monodisperse water soluble iron oxide
nanocrystals with high values of the specific absorption rate. J Mater Chem B 2(28):4426–4434.
https ://doi.org/10.1039/C4TB0 0061G
50. Kim BH, Lee N, Kim H, An K, Park YI, Choi Y, Shin K, Lee Y, Kwon SG, Na HB, Park J-G,
Ahn T-Y, Kim Y-W, Moon WK, Choi SH, Hyeon T (2011) Large-scale synthesis of uniform and
extremely small-sized iron oxide nanoparticles for high-resolution T1 magnetic resonance imaging
contrast agents. J Am Chem Soc 133(32):12624–12631. https ://doi.org/10.1021/ja203 340u
51. Kovalenko MV, Bodnarchuk MI, Lechner RT, Hesser G, Schäffler F, Heiss W (2007) Fatty acid
salts as stabilizers in size- and shape-controlled nanocrystal synthesis: the case of inverse spinel
iron oxide. J Am Chem Soc 129(20):6352–6353. https ://doi.org/10.1021/ja069 2478
52. Mourdikoudis S, Liz-Marzán LM (2013) Oleylamine in nanoparticle synthesis. Chem Mater
25(9):1465–1476. https ://doi.org/10.1021/cm400 0476
53. Hou Y, Xu Z, Sun S (2007) Controlled synthesis and chemical conversions of FeO nanoparticles.
Angew Chem Int Ed 46(33):6329–6332. https ://doi.org/10.1002/anie.20070 1694
54. Nemati Z, Alonso J, Rodrigo I, Das R, Garaio E, García JÁ, Orue I, Phan M-H, Srikanth H (2018)
Improving the heating efficiency of iron oxide nanoparticles by tuning their shape and size. J Phys
Chem C 122(4):2367–2381. https ://doi.org/10.1021/acs.jpcc.7b105 28
55. Park J, Lee E, Hwang N-M, Kang M, Kim SC, Hwang Y, Park J-G, Noh H-J, Kim J-Y, Park J-H,
Hyeon T (2005) One-nanometer-scale size-controlled synthesis of monodisperse magnetic iron
oxide nanoparticles. Angew Chem Int Ed 44(19):2872–2877. https ://doi.org/10.1002/anie.20046
1665
56. Li Z, Sun Q, Gao M (2005) Preparation of water-soluble magnetite nanocrystals from hydrated ferric salts in 2-pyrrolidone: mechanism leading to Fe 3 O 4 . Angew Chem Int Ed 44(1):123–126. https
://doi.org/10.1002/anie.20046 0715
57. Xu Z, Shen C, Hou Y, Gao H, Sun S (2009) Oleylamine as both reducing agent and stabilizer in a
facile synthesis of magnetite nanoparticles. Chem Mater 21(9):1778–1780. https ://doi.org/10.1021/
cm802 978z
58. Yang H, Ogawa T, Hasegawa D, Takahashi M (2008) Synthesis and magnetic properties of monodisperse magnetite nanocubes. J Appl Phys 103(7):07D526. https ://doi.org/10.1063/1.28338 20
59. Mohapatra J, Mitra A, Bahadur D, Aslam M (2013) Surface controlled synthesis of MFe 2 O 4
(M = Mn, Fe Co, Ni and Zn) nanoparticles and their magnetic characteristics. CrystEngComm
15(3):524–532. https ://doi.org/10.1039/C2CE2 5957E
60. Macdonald JE, Brooks CJ, Veinot JGC (2008) The influence of trace water concentration on iron
oxide nanoparticle size. Chem Commun 32:3777–3779. https ://doi.org/10.1039/B8057 15J
61. Unni M, Uhl AM, Savliwala S, Savitzky BH, Dhavalikar R, Garraud N, Arnold DP, Kourkoutis LF,
Andrew JS, Rinaldi C (2017) Thermal decomposition synthesis of iron oxide nanoparticles with
diminished magnetic dead layer by controlled addition of oxygen. ACS Nano 11(2):2284–2303.
https ://doi.org/10.1021/acsna no.7b006 09
62. Li Z, Chen H, Bao H, Gao M (2004) One-pot reaction to synthesize water-soluble magnetite
nanocrystals. Chem Mater 16(8):1391–1393. https ://doi.org/10.1021/cm035 346y
63. Ooi F, DuChene JS, Qiu J, Graham JO, Engelhard MH, Cao G, Gai Z, Wei WD (2015) A facile
solvothermal synthesis of octahedral Fe 3 O 4 nanoparticles. Small 11(22):2649–2653. https ://doi.
org/10.1002/smll.20140 1954
64. Bunge A, Porav AS, Borodi G, Radu T, Pîrnău A, Berghian-Grosan C, Turcu R (2019) Correlation
between synthesis parameters and properties of magnetite clusters prepared by solvothermal polyol
method. J Mater Sci 54(4):2853–2875. https ://doi.org/10.1007/s1085 3-018-3030-9
65. Mao B, Kang Z, Wang E, Lian S, Gao L, Tian C, Wang C (2006) Synthesis of magnetite octahedrons from iron powders through a mild hydrothermal method. Mater Res Bull 41(12):2226–2231.
https ://doi.org/10.1016/j.mater resbu ll.2006.04.037
66. Giri J, Guha Thakurta S, Bellare J, Kumar Nigam A, Bahadur D (2005) Preparation and characterization of phospholipid stabilized uniform sized magnetite nanoparticles. J Magn Magn Mater
293(1):62–68. https ://doi.org/10.1016/j.jmmm.2005.01.044
77
Reprinted from the journal