59. Fabbiani FPA, Buth G, Dittrich B, Sowa H (2010) Pressure-induced structural changes in wet
vitamin B12. CrystEngComm 12:2541
60. Grzechnik A, Meven M, Friese K (2018) Single-crystal neutron diffraction in diamond anvil
cells with hot neutrons. J Appl Crystallogr 51:351–356
61. Haberl B, Dissanayake S, Wu Y et al (2018) Next-generation diamond cell and applications to
single-crystal neutron diffraction. Rev Sci Instrum 89:092902
62. Binns J, Kamenev KV, McIntyre GJ, Moggach SA, Parsons S (2016) Use of a miniature
diamond-anvil cell in high-pressure single-crystal neutron Laue diffraction. IUCrJ 3:168–179
63. Akella J, Kennedy GC (1971) Phase diagram of benzene to 35 kbar. J Chem Phys 55:793
64. Lomberget T, Chataigner I, Bouyssi D, Maddaluno J, Balme G (2004) Diels–Alder cycloadditions of functionalized (Z)-1-benzylidene-2-methylene cyclohexanes: the beneficial effect of
high pressure. Tetrahedron Lett 45:3437–3441
65. Hutchison IB, Bull CL, Marshall WG, Parsons S, Urquhart AJ, Oswald IDH (2017) Compression of glycolide-h4 to 6GPa. Acta Crystallogr Sect B Struct Sci Cryst Eng Mater
73:1151–1157
66. Ward MR, Younis S, Cruz-Cabeza AJ, Bull CL, Funnell NP, Oswald IDH (2019) Discovery
and recovery of delta p -aminobenzoic acid. CrystEngComm 21:2058–2066
67. Zieliński W, Katrusiak A (2015) Hydrate smaller than the anhydrate. CrystEngComm
17:5468–5473
68. Millar DIA, Oswald IDH, Barry C, Francis DJ, Marshall WG, Pulham CR, Cumming AS
(2010) Pressure-cooking of explosives - the crystal structure of ε-RDX as determined by X-ray
and neutron diffraction. Chem Commun 46:5662–5664
69. Wang W, Fortes AD, Dobson DP, Howard CM, Bowles J, Hughes NJ, Wood IG (2018)
Investigation of high-pressure planetary ices by cryo-recovery. II. High-pressure apparatus,
examples and a new high-pressure phase of MgSO 4 Á5H 2 O. J Appl Crystallogr 51:692–705
70. Hutchison IB, Delori A, Wang X, Kamenev KV, Urquhart AJ, Oswald IDH (2015) Polymorphism of a polymer precursor: metastable glycolide polymorph recovered via large scale highpressure experiments. CrystEngComm 17:1778–1782
71. Wood IG, Fortes AD, Dobson DP, Wang W, Pajdzik L, Cosier J (2018) Investigation of highpressure planetary ices by cryo-recovery. I. An apparatus for X-ray powder diffraction from
40 to 315 K, allowing `cold loading’ of samples. J Appl Crystallogr 51:685–691
72. Roszak K, Katrusiek A, Katrusiak A (2016) High-pressure preference for the low Z
0 polymorph of a molecular crystal. Cryst Growth Des 16:3947–3953
73. Yan TT, Xi DY, Wang JH, Fan XF, Wan Y, Zhang LX, Wang K (2019) High-pressureinduced phase transition in cinchomeronic acid polycrystalline form-I. Chinese Phys B
28:16104
74. Abbas N, Oswald IDH, Pulham CR (2017) Accessing mefenamic acid form II through highpressure recrystallisation. Pharmaceutics 9:16
75. Cosier J, Glazer AM (1986) A nitrogen-gas-stream cryostat for general X-ray diffraction
studies. J Appl Crystallogr 19:105–107
76. Brock CP, Duncan LL (1994) Anomalous space-group frequencies for monoalcohols
CnHmOH. Chem Mater 6:1307–1312
77. McGregor PA, Allan DR, Parsons S, Pulham CR (2005) The low-temperature and highpressure crystal structures of cyclobutanol (C4H7OH). Acta Crystallogr Sect B Struct Sci
61:449–454
78. Moggach SA, Allan DR, Lozano-Casal P, Parsons S (2005) High-pressure polymorphism of
cyclopentanol (C5H10O): the structure of cyclopentanol phase-V at 1.5 GPa. J Synchrotron
Radiat 12:590–597
79. Mcgregor PA, Allan DR, Parsons S, Clark SJ (2006) Structural science hexamer formation in
tertiary butyl alcohol (2-methyl-2-propanol, C 4 H 10 O). Res Pap Acta Cryst 62:599–605
80. Oswald IDH, Allan DR, Day GM, Motherwell WDS, Parsons S (2005) Realizing predicted
crystal structures at extreme conditions: the low-temperature and high-pressure crystal structures of 2-chlorophenol and 4-fluorophenol. Cryst Growth Des 5:1055–1071
192
S. A. Moggach and I. D. H. Oswald
vitamin B12. CrystEngComm 12:2541
60. Grzechnik A, Meven M, Friese K (2018) Single-crystal neutron diffraction in diamond anvil
cells with hot neutrons. J Appl Crystallogr 51:351–356
61. Haberl B, Dissanayake S, Wu Y et al (2018) Next-generation diamond cell and applications to
single-crystal neutron diffraction. Rev Sci Instrum 89:092902
62. Binns J, Kamenev KV, McIntyre GJ, Moggach SA, Parsons S (2016) Use of a miniature
diamond-anvil cell in high-pressure single-crystal neutron Laue diffraction. IUCrJ 3:168–179
63. Akella J, Kennedy GC (1971) Phase diagram of benzene to 35 kbar. J Chem Phys 55:793
64. Lomberget T, Chataigner I, Bouyssi D, Maddaluno J, Balme G (2004) Diels–Alder cycloadditions of functionalized (Z)-1-benzylidene-2-methylene cyclohexanes: the beneficial effect of
high pressure. Tetrahedron Lett 45:3437–3441
65. Hutchison IB, Bull CL, Marshall WG, Parsons S, Urquhart AJ, Oswald IDH (2017) Compression of glycolide-h4 to 6GPa. Acta Crystallogr Sect B Struct Sci Cryst Eng Mater
73:1151–1157
66. Ward MR, Younis S, Cruz-Cabeza AJ, Bull CL, Funnell NP, Oswald IDH (2019) Discovery
and recovery of delta p -aminobenzoic acid. CrystEngComm 21:2058–2066
67. Zieliński W, Katrusiak A (2015) Hydrate smaller than the anhydrate. CrystEngComm
17:5468–5473
68. Millar DIA, Oswald IDH, Barry C, Francis DJ, Marshall WG, Pulham CR, Cumming AS
(2010) Pressure-cooking of explosives - the crystal structure of ε-RDX as determined by X-ray
and neutron diffraction. Chem Commun 46:5662–5664
69. Wang W, Fortes AD, Dobson DP, Howard CM, Bowles J, Hughes NJ, Wood IG (2018)
Investigation of high-pressure planetary ices by cryo-recovery. II. High-pressure apparatus,
examples and a new high-pressure phase of MgSO 4 Á5H 2 O. J Appl Crystallogr 51:692–705
70. Hutchison IB, Delori A, Wang X, Kamenev KV, Urquhart AJ, Oswald IDH (2015) Polymorphism of a polymer precursor: metastable glycolide polymorph recovered via large scale highpressure experiments. CrystEngComm 17:1778–1782
71. Wood IG, Fortes AD, Dobson DP, Wang W, Pajdzik L, Cosier J (2018) Investigation of highpressure planetary ices by cryo-recovery. I. An apparatus for X-ray powder diffraction from
40 to 315 K, allowing `cold loading’ of samples. J Appl Crystallogr 51:685–691
72. Roszak K, Katrusiek A, Katrusiak A (2016) High-pressure preference for the low Z
0 polymorph of a molecular crystal. Cryst Growth Des 16:3947–3953
73. Yan TT, Xi DY, Wang JH, Fan XF, Wan Y, Zhang LX, Wang K (2019) High-pressureinduced phase transition in cinchomeronic acid polycrystalline form-I. Chinese Phys B
28:16104
74. Abbas N, Oswald IDH, Pulham CR (2017) Accessing mefenamic acid form II through highpressure recrystallisation. Pharmaceutics 9:16
75. Cosier J, Glazer AM (1986) A nitrogen-gas-stream cryostat for general X-ray diffraction
studies. J Appl Crystallogr 19:105–107
76. Brock CP, Duncan LL (1994) Anomalous space-group frequencies for monoalcohols
CnHmOH. Chem Mater 6:1307–1312
77. McGregor PA, Allan DR, Parsons S, Pulham CR (2005) The low-temperature and highpressure crystal structures of cyclobutanol (C4H7OH). Acta Crystallogr Sect B Struct Sci
61:449–454
78. Moggach SA, Allan DR, Lozano-Casal P, Parsons S (2005) High-pressure polymorphism of
cyclopentanol (C5H10O): the structure of cyclopentanol phase-V at 1.5 GPa. J Synchrotron
Radiat 12:590–597
79. Mcgregor PA, Allan DR, Parsons S, Clark SJ (2006) Structural science hexamer formation in
tertiary butyl alcohol (2-methyl-2-propanol, C 4 H 10 O). Res Pap Acta Cryst 62:599–605
80. Oswald IDH, Allan DR, Day GM, Motherwell WDS, Parsons S (2005) Realizing predicted
crystal structures at extreme conditions: the low-temperature and high-pressure crystal structures of 2-chlorophenol and 4-fluorophenol. Cryst Growth Des 5:1055–1071
192
S. A. Moggach and I. D. H. Oswald