N
X
C
Hal
O
N
S
P Si
Natural
Products
Solvents
C
C
C
C C
C
251
5.14 Spectra of Solvents and References
251 251
5.14 Spectra of Solvents and References
251
5.14 Spectra of Solvents and Reference Compounds
5.14.1 1 H NMR Spectra of Common Deuterated Solvents
500 MHz; ≈1 000 data points per 1 ppm; δ in ppm relative to TMS
Acetone-d 6
10
9
8
7
6
5
4
3
2
1
0
2.10 2.05 2.00
2.05
≈2.8 (H 2 O)
Acetonitrile-d 3
10
9
8
7
6
5
4
3
2
1
0
2.00 1.95 1.90
1.94
2.09 (H 2 O)
Benzene-d 6 
10
9
8
7
6
5
4
3
2
1
0
7.16
Bromoform-d
10
9
8
7
6
5
4
3
2
1
0
6.84
Chloroform-d
10
9
8
7
6
5
4
3
2
1
0
7.26
1.55 (H 2 O)