N
X
C
O
N
S
Hal
Solvents
Natural
Products
P Si
C
C
C C
C
C
130
4 13 C NMR
4.10 Sulfur Compounds
4.10.1 Thiols
13 C Chemical Shifts (δ in ppm)
4.10.2 Sulfides
13 C Chemical Shifts (δ in ppm)
H 3 C S
S
S
S
H 3 C
CH 3
H 3 C
S
S
H 3 C S
CH 3
S
S
S
CH 3 SH
SH
SH
SH
SH
SH
SH
SH
SH
HS
SH
HO
SH
SH
SH
SH
SH
6.5
19.7
27.6
27.4
12.6
21.0
30.6
14.0
12.0
14.0
22.6
13.7
22.2
31.8
38.8
28.1
26.4
23.7
24.6
35.7
31.4
22.0
34.1
15.5
34.1
34.1
22.0
54.8
14.4
59.2
43.1
38.3
38.5
28.8
130.6
141.0
129.2
127.9
125.3
126.8
128.8
128.5
38.5
26.8
25.9
37.7
24.6
19.3
28.7
64.2
27.3
28.1
31.4
23.2
31.4
30.4
30.9
13.7
33.2
45.6
24.7
35.0
33.9
41.1
29.9
19.1
S
S
S
S
23.2
14.8
34.3
25.5
33.4
23.6
13.7
28.0