2.7 Experimental Section
73
40
35
30
25
20
15
10
5
2θ / º
3/CHCl 3
3/Py
3/CH 2 Cl 2
3/CH 2 Br 2
3/DMA
3/AcH
3/CH 3 CN
3/DMF
3/SPO
3/racPO
3/acetone
3/none
Intensity
Fig. 2.40 Simulated powder patterns derived from the single crystals of 3/solvent and 3/none, in
which 3/solvent corresponds to 3/CHCl 3 , 3/Py, 3/CH 2 Cl 2 , 3/CH 2 Br 2 , 3/DMA, 3/AcH, 3/CH 3 CN,
3/DMF, 3/SPO, 3/racPO, and 3/acetone