2.7 Experimental Section
41
Fig. 2.18 1 H NMR spectra of a 3/CHCl 3 in CD 2 Cl 2 and ten 3/solvent in CDCl 3 , in which b 3/Py,
c 3/CH 2 Cl 2 , d 3/CH 2 Br 2 , e 3/DMA, f 3/AcH, g 3/CH 3 CN, h 3/DMF, i 3/SPO, j 3/racPO, and k
3/acetone are obtained by solvent addition to 3 ground . Arrows indicate that proton signals attributed
to included solvent molecules
41
Fig. 2.18 1 H NMR spectra of a 3/CHCl 3 in CD 2 Cl 2 and ten 3/solvent in CDCl 3 , in which b 3/Py,
c 3/CH 2 Cl 2 , d 3/CH 2 Br 2 , e 3/DMA, f 3/AcH, g 3/CH 3 CN, h 3/DMF, i 3/SPO, j 3/racPO, and k
3/acetone are obtained by solvent addition to 3 ground . Arrows indicate that proton signals attributed
to included solvent molecules