salt, furosemide, pravastatin
sodium salt, carbamazepine,
nimesulide, (Æ)-metoprolol,
(Æ)-tartrate salt, clotrimazole, trimethoprim, caffeine,
S(Æ)-2-(6-methoxy-2naphthyl)-propionic acid
(naproxen), and irgasan
(triclosan)
Acetaminophen, diclofenac,
fenoprofen, ibuprofen, indomethacin, ketoprofen,
mefenamic acid, naproxen,
phenazone, bezafibrate,
clofibric acid, gemfibrozil,
pravastatin, caffeine, carbamazepine, famotidine, ranitidine, atenolol, metoprolol,
nadolol, pindolol, propranolol, timolol, furosemide,
hydrochlorothiazide,
glyburide, albuterol, chloramphenicol, clindamycin,
flumequine, lincomycin,
metronidazole, novobiocin,
ornidazole, sulfadiazine,
sulfadimethoxine,
sulfaguanidine,
sulfamethazine,
sulfamethizole, sulfamethoxazole,
sulfamethoxypyridazine,
sulfanilamide, sulfathiazole,
sulfisoxazole, trimethoprim
4 g
Milli-Q water at
neutral pH
100
C
1,500 psi
5 min
 3
60%
Hydromatrix
HLB
cartridges
50–140%
Not
reported
<0.01–
0.83 ng/g
UPLC-MS/
MS
[53]
Sulfapyridine,
sulfamerazine,
sulfadimethoxine, tetracycline, chlortetracycline, oxytetracycline, doxycycline,
erythromycin,
roxithromycin
3 g
50% phosphate
buffer and 50%
acetonitrile with
pH
¼ 3
70
C
1,500 psi
10 min
 1
60%
Diatomite
Tandem
SAX-HLB
SPE
cartridges
60.2–97.6%
<10%
0.2–1.7
μg/kg
HPLC-MS/
MS
[70]
Sulfapyridine,
sulfamerazine,
sulfadimoxine, tetracycline,
chlortetracycline,
3 g
50% methanol
and 50% 0.2 M
citric acid with
70
C
1,500 psi
10 min
 1
60%
Sea sand and
diatomite
Tandem
SAX-HLB
SPE
cartridges
67.3–97.4%
<9%
0.2–1.1 ug/kg
HPLC-MS/
MS
[71]
(continued)
Development of Methods for the Determination of PhACs in Soil/Earthworm/Crop. . .
427