1 3
Topics in Current Chemistry (2020) 378:2
114. Marchand R, Brohan L, Tournoux M (1980) TiO 2 (B) a new form of titanium dioxide and the
potassium octatitanate K 2 Ti 8 O 17 . Mater Res Bull 15:1129–1133. https ://doi.org/10.1016/00255408(80)90076 -8
115. Joo J, Kwon SG, Yu T et al (2005) Large-scale synthesis of TiO 2 nanorods via nonhydrolytic sol−
gel ester elimination reaction and their application to photocatalytic inactivation of E. coli. J Phys
Chem B 109:15297–15302. https ://doi.org/10.1021/jp052 458z
116. Ma Y, Lin Y, Xiao X et al (2006) Sonication–hydrothermal combination technique for the synthesis of titanate nanotubes from commercially available precursors. Mater Res Bull 41:237–243.
https ://doi.org/10.1016/j.mater resbu ll.2005.08.020
117. Viriya-empikul N, Charinpanitkul T, Sano N et al (2009) Effect of preparation variables on morphology and anatase-brookite phase transition in sonication assisted hydrothermal reaction for synthesis of titanate nanostructures. Mater Chem Phys 118:254–258. https ://doi.org/10.1016/j.match
emphy s.2009.07.042
118. Viriya-Empikul N, Sano N, Charinpanitkul T et al (2008) A step towards length control of titanate
nanotubes using hydrothermal reaction with sonication pretreatment. Nanotechnology. https ://doi.
org/10.1088/0957-4484/19/03/03560 1
119. Begin-Colin S, Le Caer G, Mocellin A, Zandona M (1994) Polymorphie transformations of titania
induced by ball milling. Philos Mag Lett 69:1–7. https ://doi.org/10.1080/09500 83940 82424 30
120. Lu CJ, Zhang J, Li ZQ (2004) Structural evolution of titanium powder during ball milling in different atmospheres. J Alloys Compd 381:278–283. https ://doi.org/10.1016/j.jallc om.2004.03.130
121. Pang P, Li W, Liu Y (2007) Effect of ball milling process on the microstructure of titaniumnanohydroxyapatite composite powder. Rare Met 26:118–123. https ://doi.org/10.1016/S1001
-0521(07)60170 -3
122. Silva CC, Graça MPF, Valente MA, Sombra ASB (2007) Crystallite size study of nanocrystalline
hydroxyapatite and ceramic system with titanium oxide obtained by dry ball milling. J Mater Sci
42:3851–3855. https ://doi.org/10.1007/s1085 3-006-0474-0
123. Bégin-Colin S, Girot T, Le Caër G, Mocellin A (2000) Kinetics and mechanisms of phase transformations induced by ball-milling in anatase TiO 2 . J Solid State Chem 149:41–48. https ://doi.
org/10.1006/jssc.1999.8491
124. Yadav BC, Singh S, Yadav TP (2015) Titania prepared by ball milling: its characterization and
application as liquefied petroleum gas sensor. Synth React Inorg Met Nano-Metal Chem 45:487–
494. https ://doi.org/10.1080/15533 174.2012.74989 2
125. Rajender G, Giri PK (2016) Strain induced phase formation, microstructural evolution and bandgap narrowing in strained TiO 2 nanocrystals grown by ball milling. J Alloys Compd 676:591–600.
https ://doi.org/10.1016/j.jallc om.2016.03.154
126. Jung HJ, Nam K, Sung HG et al (2016) Preparation of TiO 2 -decorated boron particles by wet
ball milling and their photoelectrochemical hydrogen and oxygen evolution reactions. Materials
(Basel). https ://doi.org/10.3390/ma912 1012
127. Billik P, Plesch G (2007) Mechanochemical synthesis of nanocrystalline TiO 2 from liquid TiCl4.
Scr Mater 56:979–982. https ://doi.org/10.1016/j.scrip tamat .2007.01.048
128. Billik P, Plesch G, Brezová V et al (2007) Anatase TiO 2 nanocrystals prepared by mechanochemical synthesis and their photochemical activity studied by EPR spectroscopy. J Phys Chem Solids
68:1112–1116. https ://doi.org/10.1016/j.jpcs.2007.02.010
129. Salari M, Rezaee M, Marashi SPH, Aboutalebi SH (2009) The role of the diluent phase in the
mechanochemical preparation of TiO 2 nanoparticles. Powder Technol 192:54–57. https ://doi.
org/10.1016/j.powte c.2008.11.011
130. Li C, Liang B, Song H et al (2008) Preparation of porous rutile titania from ilmenite by mechanical
activation and subsequent sulfuric acid leaching. Microporous Mesoporous Mater 115:293–300.
https ://doi.org/10.1016/j.micro meso.2008.01.045
131. Tao T, Glushenkov AM, Liu H et al (2011) Ilmenite FeTiO 3 nanoflowers and their pseudocapacitance. J Phys Chem C 115:17297–17302. https ://doi.org/10.1021/jp203 345s
132. Yu J, Chen Y (2010) One-dimensional growth of TiO 2 nanorods from ilmenite sands. J Alloys
Compd 504:S364–S367. https ://doi.org/10.1016/j.jallc om.2010.02.145
133. Yu J, Chen Y, Glushenkov AM (2009) Titanium oxide nanorods extracted from ilmenite sands.
Cryst Growth Des 9:1240–1244. https ://doi.org/10.1021/cg801 125w
134. Tao T, Chen Y, Zhou D et al (2013) Expanding the applications of the ilmenite mineral to the
preparation of nanostructures: TiO 2 nanorods and their photocatalytic properties in the degradation
of oxalic acid. Chem A Eur J 19:1091–1096. https ://doi.org/10.1002/chem.20120 2451
69
Reprinted from the journal
Topics in Current Chemistry (2020) 378:2
114. Marchand R, Brohan L, Tournoux M (1980) TiO 2 (B) a new form of titanium dioxide and the
potassium octatitanate K 2 Ti 8 O 17 . Mater Res Bull 15:1129–1133. https ://doi.org/10.1016/00255408(80)90076 -8
115. Joo J, Kwon SG, Yu T et al (2005) Large-scale synthesis of TiO 2 nanorods via nonhydrolytic sol−
gel ester elimination reaction and their application to photocatalytic inactivation of E. coli. J Phys
Chem B 109:15297–15302. https ://doi.org/10.1021/jp052 458z
116. Ma Y, Lin Y, Xiao X et al (2006) Sonication–hydrothermal combination technique for the synthesis of titanate nanotubes from commercially available precursors. Mater Res Bull 41:237–243.
https ://doi.org/10.1016/j.mater resbu ll.2005.08.020
117. Viriya-empikul N, Charinpanitkul T, Sano N et al (2009) Effect of preparation variables on morphology and anatase-brookite phase transition in sonication assisted hydrothermal reaction for synthesis of titanate nanostructures. Mater Chem Phys 118:254–258. https ://doi.org/10.1016/j.match
emphy s.2009.07.042
118. Viriya-Empikul N, Sano N, Charinpanitkul T et al (2008) A step towards length control of titanate
nanotubes using hydrothermal reaction with sonication pretreatment. Nanotechnology. https ://doi.
org/10.1088/0957-4484/19/03/03560 1
119. Begin-Colin S, Le Caer G, Mocellin A, Zandona M (1994) Polymorphie transformations of titania
induced by ball milling. Philos Mag Lett 69:1–7. https ://doi.org/10.1080/09500 83940 82424 30
120. Lu CJ, Zhang J, Li ZQ (2004) Structural evolution of titanium powder during ball milling in different atmospheres. J Alloys Compd 381:278–283. https ://doi.org/10.1016/j.jallc om.2004.03.130
121. Pang P, Li W, Liu Y (2007) Effect of ball milling process on the microstructure of titaniumnanohydroxyapatite composite powder. Rare Met 26:118–123. https ://doi.org/10.1016/S1001
-0521(07)60170 -3
122. Silva CC, Graça MPF, Valente MA, Sombra ASB (2007) Crystallite size study of nanocrystalline
hydroxyapatite and ceramic system with titanium oxide obtained by dry ball milling. J Mater Sci
42:3851–3855. https ://doi.org/10.1007/s1085 3-006-0474-0
123. Bégin-Colin S, Girot T, Le Caër G, Mocellin A (2000) Kinetics and mechanisms of phase transformations induced by ball-milling in anatase TiO 2 . J Solid State Chem 149:41–48. https ://doi.
org/10.1006/jssc.1999.8491
124. Yadav BC, Singh S, Yadav TP (2015) Titania prepared by ball milling: its characterization and
application as liquefied petroleum gas sensor. Synth React Inorg Met Nano-Metal Chem 45:487–
494. https ://doi.org/10.1080/15533 174.2012.74989 2
125. Rajender G, Giri PK (2016) Strain induced phase formation, microstructural evolution and bandgap narrowing in strained TiO 2 nanocrystals grown by ball milling. J Alloys Compd 676:591–600.
https ://doi.org/10.1016/j.jallc om.2016.03.154
126. Jung HJ, Nam K, Sung HG et al (2016) Preparation of TiO 2 -decorated boron particles by wet
ball milling and their photoelectrochemical hydrogen and oxygen evolution reactions. Materials
(Basel). https ://doi.org/10.3390/ma912 1012
127. Billik P, Plesch G (2007) Mechanochemical synthesis of nanocrystalline TiO 2 from liquid TiCl4.
Scr Mater 56:979–982. https ://doi.org/10.1016/j.scrip tamat .2007.01.048
128. Billik P, Plesch G, Brezová V et al (2007) Anatase TiO 2 nanocrystals prepared by mechanochemical synthesis and their photochemical activity studied by EPR spectroscopy. J Phys Chem Solids
68:1112–1116. https ://doi.org/10.1016/j.jpcs.2007.02.010
129. Salari M, Rezaee M, Marashi SPH, Aboutalebi SH (2009) The role of the diluent phase in the
mechanochemical preparation of TiO 2 nanoparticles. Powder Technol 192:54–57. https ://doi.
org/10.1016/j.powte c.2008.11.011
130. Li C, Liang B, Song H et al (2008) Preparation of porous rutile titania from ilmenite by mechanical
activation and subsequent sulfuric acid leaching. Microporous Mesoporous Mater 115:293–300.
https ://doi.org/10.1016/j.micro meso.2008.01.045
131. Tao T, Glushenkov AM, Liu H et al (2011) Ilmenite FeTiO 3 nanoflowers and their pseudocapacitance. J Phys Chem C 115:17297–17302. https ://doi.org/10.1021/jp203 345s
132. Yu J, Chen Y (2010) One-dimensional growth of TiO 2 nanorods from ilmenite sands. J Alloys
Compd 504:S364–S367. https ://doi.org/10.1016/j.jallc om.2010.02.145
133. Yu J, Chen Y, Glushenkov AM (2009) Titanium oxide nanorods extracted from ilmenite sands.
Cryst Growth Des 9:1240–1244. https ://doi.org/10.1021/cg801 125w
134. Tao T, Chen Y, Zhou D et al (2013) Expanding the applications of the ilmenite mineral to the
preparation of nanostructures: TiO 2 nanorods and their photocatalytic properties in the degradation
of oxalic acid. Chem A Eur J 19:1091–1096. https ://doi.org/10.1002/chem.20120 2451
69
Reprinted from the journal