A
B
105
Downfield
backbone NH
1 1
1 0
9
8
7
6
5
4
3
2
1
0
- 1
- 2
p p m
Upfield
CH 3
Downfield
Hα
110
115
120
125
130
10.0
9.5
9.0
8.5
8.0
7.5
7.0
15
N (ppm)
1 H (ppm)
1 H (ppm)
Fig. 6 NMR spectra of MAST2-PDZ. (a)
1
H 1D spectrum of 150 μM MAST2-PDZ
in complex with a viral peptide at 600 MHz 1H frequency. (b)
1
H15
N 2D HSQC
spectra of 150 μM MAST2-PDZ alone (in black) and in complex with a viral
peptide (in red) at 600 MHz
1
H frequency
102
Ce ´ lia Caillet-Saguy et al.
B
105
Downfield
backbone NH
1 1
1 0
9
8
7
6
5
4
3
2
1
0
- 1
- 2
p p m
Upfield
CH 3
Downfield
Hα
110
115
120
125
130
10.0
9.5
9.0
8.5
8.0
7.5
7.0
15
N (ppm)
1 H (ppm)
1 H (ppm)
Fig. 6 NMR spectra of MAST2-PDZ. (a)
1
H 1D spectrum of 150 μM MAST2-PDZ
in complex with a viral peptide at 600 MHz 1H frequency. (b)
1
H15
N 2D HSQC
spectra of 150 μM MAST2-PDZ alone (in black) and in complex with a viral
peptide (in red) at 600 MHz
1
H frequency
102
Ce ´ lia Caillet-Saguy et al.