CARBON-CARBON BOND FORMING REACTIONS
77
I.B.2.b-4 Lange, G.L. and Gottardo, C , TL, 35, 8513; see also:
Banwell, M.G. and Dupuche, J.R., AJC, 47, 203; Ranu, B.C. and Das,
A.R., JCS(Pl), 921.
Bu 3 SnH, AIBN
Ph-H
0 " Λ
/ " O C S 2 M e
^ o «
92%
I.B.2.b-5 Duhamel, P. et al., TL, 35, 1209.
OH
+
OMe
Cl
BF 3 «Et 2 0
'PrOH/EtN0 2 , -30°C
CHO
Cl
DBU
CH 2 CI 2 , 50°C, 2h
CHO
86%
77
I.B.2.b-4 Lange, G.L. and Gottardo, C , TL, 35, 8513; see also:
Banwell, M.G. and Dupuche, J.R., AJC, 47, 203; Ranu, B.C. and Das,
A.R., JCS(Pl), 921.
Bu 3 SnH, AIBN
Ph-H
0 " Λ
/ " O C S 2 M e
^ o «
92%
I.B.2.b-5 Duhamel, P. et al., TL, 35, 1209.
OH
+
OMe
Cl
BF 3 «Et 2 0
'PrOH/EtN0 2 , -30°C
CHO
Cl
DBU
CH 2 CI 2 , 50°C, 2h
CHO
86%