USEFUL SYNTHETIC PREPARATIONS
VI.C. Nucleotides. Etc.
383
VI.C-1 Reddy, M.P. et al., 7X, 35, 5771; Pedroso, E. et al., T, 50, 2617;
Beaucage, S.L. et al., JOC, 59, 1963; see also: Rao, M.V. and Macfarlane,
K., TL, 35, 6741.
New and Efficient Solid Support for the Synthesis of Nucleic Acids.
VI.C-2 Sujino, K. and Sugimura, H., CC, 2541; Mevellec, L. and Huet, F.,
Γ,50, 13145.
OMe
N ^ ι
1: Me2S(SMe)BF 4
-°^J[ JL
MeCN, -20°C *" O^^N^^OMe
O
Ν ^ Ί Μ β 2:NaOH H Q
]
^
K=J
SPh
VI.C-3 Jung, M.E. and Rhee, H., JOC, 59,4719; Schneller, S.W. et al.,
./MC, 37, 551.
α
AcO
NTs 2 \ - ^ A
Ac<
IN
N ^ N H 2
Na
Pd[P(Oi'Pr) 3 ] 4
NH 2
68%