USEFUL SYNTHETIC PREPARATIONS
375
VI.A.13-4 Sonawane, H.R. et al., CC, 1215.
H 2 Q 2 ,TS-1, acetone, A
^ ^ N
ArNH 2
*»
N
Ar
I
Ar 10-75 %
TS-1 = titanium silicate zeolite
VI.A.13-5 Dondoni, A. et al., SC, 24, 2537 and 2551.
O,
RCHO + BnNHOH
MgSQ 4 , CH 2 CI 2>
^ N < ^ R
Bn 59-90 %
VI.A.13-6 Huang, H.C. et al., TI, 35, 7201.
Ο ^ ^ Ο
1; MeMgCI
R ^ M e
2 : B B u 3
3: H 2 NOS0 3 H
R
NH 2
36-67 %
VI.A.13-7 Olah, G.A., Prakash, G.K.S. et al., S, 468; Patel, H.V. et al.,
OPP, 26, 118; Suzuki, H. et al., JCS(Pl), 903, 1367 and S, 841; Evans,
P.A. and Longmire, J.M., TL, 35, 8345; Bakke, J.M. and Hegbom, I., ACS,
48, 181; Hwu, J.R. et al., CC, 1425; see also: Bosch, E. and Kochi, J.K.,
JOC, 59, 5573.
^ χ '
NaNQ 3 , TMSCI, A1C1 3
62-97 %
N 0 2
375
VI.A.13-4 Sonawane, H.R. et al., CC, 1215.
H 2 Q 2 ,TS-1, acetone, A
^ ^ N
ArNH 2
*»
N
Ar
I
Ar 10-75 %
TS-1 = titanium silicate zeolite
VI.A.13-5 Dondoni, A. et al., SC, 24, 2537 and 2551.
O,
RCHO + BnNHOH
MgSQ 4 , CH 2 CI 2>
^ N < ^ R
Bn 59-90 %
VI.A.13-6 Huang, H.C. et al., TI, 35, 7201.
Ο ^ ^ Ο
1; MeMgCI
R ^ M e
2 : B B u 3
3: H 2 NOS0 3 H
R
NH 2
36-67 %
VI.A.13-7 Olah, G.A., Prakash, G.K.S. et al., S, 468; Patel, H.V. et al.,
OPP, 26, 118; Suzuki, H. et al., JCS(Pl), 903, 1367 and S, 841; Evans,
P.A. and Longmire, J.M., TL, 35, 8345; Bakke, J.M. and Hegbom, I., ACS,
48, 181; Hwu, J.R. et al., CC, 1425; see also: Bosch, E. and Kochi, J.K.,
JOC, 59, 5573.
^ χ '
NaNQ 3 , TMSCI, A1C1 3
62-97 %
N 0 2