218
ORGANIC SYNTHESIS—1995
III.F.3. C-S -> C-H
IILF.3-1 Hamel, P. et al., JOC, 59, 6372; Hosomi, A. et al., BCJ, 67,
1495; Yamakawa, K. et al., T, 50,4957.
SR3
III.F.3-2 Hansen, M.M. and Harkness, A.R., TL, 35, 6971.
O
R
O
R
^
Zn, HOAc, Δ
NH
—»►
NH
59-90 %
III.F.3-3 Kurihara, T. et al., TL, 35, 1255.
-O
OTBS
s
SmI 2 ,THF
Γ ^
I
HMPA, rt < ■ ^
4
/*^o
OH
78%
-OTBS
ORGANIC SYNTHESIS—1995
III.F.3. C-S -> C-H
IILF.3-1 Hamel, P. et al., JOC, 59, 6372; Hosomi, A. et al., BCJ, 67,
1495; Yamakawa, K. et al., T, 50,4957.
SR3
III.F.3-2 Hansen, M.M. and Harkness, A.R., TL, 35, 6971.
O
R
O
R
^
Zn, HOAc, Δ
NH
—»►
NH
59-90 %
III.F.3-3 Kurihara, T. et al., TL, 35, 1255.
-O
OTBS
s
SmI 2 ,THF
Γ ^
I
HMPA, rt < ■ ^
4
/*^o
OH
78%
-OTBS